4-benzoyl-6-chlororesorcinol

Base Information

• Chemical Name: 4-benzoyl-6-chlororesorcinol
• CAS No.: 3286-95-1
• Molecular Formula: C₁₃H₉ClO₃
• Molecular Weight: 248.666
• Mol file: 3286-95-1.mol

Synonyms:

Chemical Property of 4-benzoyl-6-chlororesorcinol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-benzoyl-6-chlororesorcinol

There total 3 articles about 4-benzoyl-6-chlororesorcinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-Dimethoxybenzene (151-10-0) → 4-benzoyl-6-chlororesorcinol (3286-95-1)

Guidance literature:

Multi-step reaction with 2 steps

1: SO₂Cl₂ / CHCl₃ / Ambient temperature

2: AlCl₃ / 1,2-dichloro-ethane / 0 deg C to RT, 3 h, then 50 deg C, 1 h

With aluminium trichloride; sulfuryl dichloride; In chloroform; 1,2-dichloro-ethane;

DOI:10.1248/cpb.40.2597

Reference yield:

1-chloro-2,4-dimethoxybenzene (7051-13-0) + benzoyl chloride (98-88-4) → 4-benzoyl-6-chlororesorcinol (3286-95-1)

Guidance literature:

With aluminium trichloride; In 1,2-dichloro-ethane; Yield given; 0 deg C to RT, 3 h, then 50 deg C, 1 h;

DOI:10.1248/cpb.40.2597

Reference yield:

→ 4-benzoyl-6-chlororesorcinol (3286-95-1)

Guidance literature:

Aus 4-Chlor-resorcinol + Benzotrichlorid;

upstream raw materials:

1-chloro-2,4-dimethoxybenzene

benzoyl chloride

1,3-Dimethoxybenzene

Downstream raw materials:

C₂₇H₂₁ClO₇S₂

4-chloro-6-(α-hydroxyiminobenzyl)-1,3-O,O-ditosylresorcinol

8-bromo-5-chloro-7,7-diethoxy-3-phenylisoxazolo<5,4-f>chroman

ethyl 2-bromo-3-5'-chloro-6'-hydroxy-3'-phenyl-1',2'-benzisoxazol-7'-ylpropionate