N-benzoyl-DL-alanine triphenyltin(IV)

Base Information

• Chemical Name: N-benzoyl-DL-alanine triphenyltin(IV)
• CAS No.: 114542-82-4
• Molecular Formula: C₂₈H₂₅NO₃Sn
• Molecular Weight: 542.221
• Mol file: 114542-82-4.mol

Synonyms:

Chemical Property of N-benzoyl-DL-alanine triphenyltin(IV)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-benzoyl-DL-alanine triphenyltin(IV)

There total 1 articles about N-benzoyl-DL-alanine triphenyltin(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

triphenyltin chloride (639-58-7) + sodium N-benzoylalaninate → N-benzoyl-DL-alanine triphenyltin(IV) (114542-82-4)

Guidance literature:

In ethanol; benzene; byproducts: NaCl; to soln. of sodium salt was added Sn compd. and refluxed for 6-8 h, then formed NaCl was filtered off and refluxing continued, this process was repeated two or three times; solvents were removed in vac. and residue recrystd. from dry benzene; elem. anal.;

DOI:10.1016/0022-328X(87)85125-2

Reference yield:

dimethylsulfoxide-d6 (2206-27-1) + N-benzoyl-DL-alanine triphenyltin(IV) (114542-82-4) → C6H5CONHCH(CH3)COOSn(C6H5)3(CD3)2SO

Guidance literature:

In dimethylsulfoxide-d6; dissoln. of Sn compd. in DMSO-d6; not isolated, detected by NMR;

DOI:10.1016/0022-328X(87)85125-2

upstream raw materials:

triphenyltin chloride