cis-dichlorobis[tris(3-methoxyphenyl)phosphane]platinum(II)

Base Information

Chemical Name:cis-dichlorobis[tris(3-methoxyphenyl)phosphane]platinum(II)
CAS No.:100448-94-0
Molecular Formula:C₄₂H₄₂Cl₂O₆P₂Pt
Molecular Weight:970.725
Hs Code.:

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Chemical Property of cis-dichlorobis[tris(3-methoxyphenyl)phosphane]platinum(II)

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Technology Process of cis-dichlorobis[tris(3-methoxyphenyl)phosphane]platinum(II)

There total 2 articles about cis-dichlorobis[tris(3-methoxyphenyl)phosphane]platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 10025-99-7
potassium tetrachloroplatinate(II)

: 29949-84-6
tris(3-methoxyphenyl)phosphine

: 100448-94-0
cis-dichlorobis[tris(3-methoxyphenyl)phosphane]platinum(II)

Guidance literature:: In xylene; N2 atmosphere; refluxed for 4 h; stirred for 16 h at room temp.;; crystals sepd.; washed with ethanol and ether; elem. anal.;

Reference yield: 43.0%

: 12080-32-9
dichloro(1,5-cyclooctadiene)platinum(ll)

: 29949-84-6
tris(3-methoxyphenyl)phosphine

: 100448-94-0
cis-dichlorobis[tris(3-methoxyphenyl)phosphane]platinum(II)

Guidance literature:: In dichloromethane; phosphane soln. added dropwise to complex soln. at room temp.; refluxedfor 1 h; solvent removed in vacuo; dissolved in CH2Cl2; layered with ether; crystn. at -20°C for 20 h; washed with CH2Cl2/ether and acetone; dried in vacuo over silica gel; elem. anal.;

Reference yield: 23.0%

: 100448-94-0
cis-dichlorobis[tris(3-methoxyphenyl)phosphane]platinum(II)

: 100569-37-7
trans-dichlorobis[tris(3-methoxyphenyl)phosphane]platinum(II)

Guidance literature:: In dichloromethane; Irradiation (UV/VIS); N2-atmosphere; irradiation (1000 W Hg high-pressure lamp) of a vigorously stirred soln. at 20°C for 72 h;; filtered; Al2O3 (neutral) added to filtrate; solvent removed in vacuo; chromy. (Al2O3, UV-detection 254 nm); first fraction concd.; layered with ether; crystals sepd. after 24 h at -20°C; washed three times with ether; elem. anal.;