1-(2-deoxy-1,3-di-N-p-tolylsulfonyl-streptamin-4-yl) 8-methyl (8R,S)-2-deoxy-2-p-tolylsulfonamido-D-threo-α-D-gluco-octodialdo-1,5:8,4-dipyranodioside

Base Information

• Chemical Name: 1-(2-deoxy-1,3-di-N-p-tolylsulfonyl-streptamin-4-yl) 8-methyl (8R,S)-2-deoxy-2-p-tolylsulfonamido-D-threo-α-D-gluco-octodialdo-1,5:8,4-dipyranodioside
• CAS No.: 92734-27-5
• Molecular Formula: C₃₆H₄₇N₃O₁₅S₃
• Molecular Weight: 857.978

Synonyms:

Chemical Property of 1-(2-deoxy-1,3-di-N-p-tolylsulfonyl-streptamin-4-yl) 8-methyl (8R,S)-2-deoxy-2-p-tolylsulfonamido-D-threo-α-D-gluco-octodialdo-1,5:8,4-dipyranodioside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(2-deoxy-1,3-di-N-p-tolylsulfonyl-streptamin-4-yl) 8-methyl (8R,S)-2-deoxy-2-p-tolylsulfonamido-D-threo-α-D-gluco-octodialdo-1,5:8,4-dipyranodioside

There total 2 articles about 1-(2-deoxy-1,3-di-N-p-tolylsulfonyl-streptamin-4-yl) 8-methyl (8R,S)-2-deoxy-2-p-tolylsulfonamido-D-threo-α-D-gluco-octodialdo-1,5:8,4-dipyranodioside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + 1-(2-deoxy-1,3-di-N-p-tolylsulfonyl-streptamin-4-yl) (8R,S)-2-deoxy-2-p-tolylsulfonamido-D-threo-α-D-gluco-octodialdo-1,5-pyranoside-8,4-pyranose (88897-33-0) → 1-(2-deoxy-1,3-di-N-p-tolylsulfonyl-streptamin-4-yl) 8-methyl (8S)-2-deoxy-2-p-tolylsulfonamido-D-threo-α-D-gluco-octodialdo-1,5:8,4-dipyranodioside (92734-27-5) + 1-(2-deoxy-1,3-di-N-p-tolylsulfonyl-streptamin-4-yl) 8-methyl (8R)-2-deoxy-2-p-tolylsulfonamido-D-threo-α-D-gluco-octodialdo-1,5:8,4-dipyranodioside (92734-27-5)

Guidance literature:

With hydrogenchloride; for 1h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Heating;

DOI:10.1016/0008-6215(84)85280-5

Reference yield:

methanol (67-56-1) + 1-(2-deoxy-1,3-di-N-p-tolylsulfonyl-streptamin-4-yl) (8R,S)-2-deoxy-2-p-tolylsulfonamido-D-threo-α-D-gluco-octodialdo-1,5-pyranoside-8,4-pyranose (88897-33-0) → 1-(2-deoxy-1,3-di-N-p-tolylsulfonyl-streptamin-4-yl) 8-methyl (8S)-2-deoxy-2-p-tolylsulfonamido-D-threo-α-D-gluco-octodialdo-1,5:8,4-dipyranodioside (92734-27-5) + 1-(2-deoxy-1,3-di-N-p-tolylsulfonyl-streptamin-4-yl) 8-methyl (8R)-2-deoxy-2-p-tolylsulfonamido-D-threo-α-D-gluco-octodialdo-1,5:8,4-dipyranodioside (92734-27-5)

Guidance literature:

With hydrogenchloride; for 1h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Heating;

DOI:10.1016/0008-6215(84)85280-5

Reference yield:

1-(2-deoxy-1,3-di-N-p-tolylsulfonyl-streptamin-4-yl) 8-methyl (8R,S)-2-deoxy-2-p-tolylsulfonamido-D-threo-α-D-gluco-octodialdo-1,5:8,4-dipyranodioside (92734-27-5) → 1-(2-deoxystreptamin-4-yl) 8-methyl (8S)-2-amino-2-deoxy-D-threo-α-D-gluco-octodialdo-1,5:8,4-dipyranodioside (92734-28-6) + 1-(2-deoxystreptamin-4-yl) 8-methyl (8R)-2-amino-2-deoxy-D-threo-α-D-gluco-octodialdo-1,5:8,4-dipyranodioide (92734-28-6)

Guidance literature:

With ammonia; sodium; ethylamine; at -65 ℃; for 1.5h; Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1016/0008-6215(84)85280-5

upstream raw materials:

methanol

1-(2-deoxy-1,3-di-N-p-tolylsulfonyl-streptamin-4-yl) (8R,S)-2-deoxy-2-p-tolylsulfonamido-D-threo-α-D-gluco-octodialdo-1,5-pyranoside-8,4-pyranose

Downstream raw materials:

1-(2-deoxystreptamin-4-yl) 8-methyl (8S)-2-amino-2-deoxy-D-threo-α-D-gluco-octodialdo-1,5:8,4-dipyranodioside

1-(2-deoxystreptamin-4-yl) 8-methyl (8R)-2-amino-2-deoxy-D-threo-α-D-gluco-octodialdo-1,5:8,4-dipyranodioide

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