W₂Cp₂(μ-PPh₂)₂(CO)₂

Base Information

Chemical Name:W₂Cp₂(μ-PPh₂)₂(CO)₂
CAS No.:910327-76-3
Molecular Formula:C₃₆H₃₀O₂P₂W₂
Molecular Weight:924.281
Hs Code.:

W<sub>2</sub>Cp<sub>2</sub>(μ-PPh<sub>2</sub>)<sub>2</sub>(CO)<sub>2</sub>

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Chemical Property of W₂Cp₂(μ-PPh₂)₂(CO)₂

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Technology Process of W₂Cp₂(μ-PPh₂)₂(CO)₂

There total 3 articles about W₂Cp₂(μ-PPh₂)₂(CO)₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 221874-66-4
[W2(μ-CO)Cp2(μ-PPh2)2]

: 201230-82-2
carbon monoxide

: 910327-76-3,483306-17-8
W₂Cp₂(μ-PPh₂)₂(CO)₂

Guidance literature:: In toluene; under N2; toluene soln. of W complex frozen (liq. N2); vac. evacuated; the tube filled with CO; closed; heated to room temp.; stirred at room temp. for 10 min; solvent removed under vac.; washed with petroleum ether; elem. anal.;
DOI:10.1021/om020573f

Reference yield: 72.0%

: 910294-15-4
[W2Cp2(μ-H)(μ-PPh2)2(CO)2]BF4

: 910327-76-3,483306-17-8
W₂Cp₂(μ-PPh₂)₂(CO)₂

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; (N2); stirred at 263 K for 1 min; evapd. (vac.), chromd. (alumina, at 285 K, CH2Cl2/petroleum ether), solvent-removed; elem. anal.;
DOI:10.1021/ic060544n

Reference yield:

: 910294-09-6
[W2Cp2(H)(μ-PPh2)2(CO)2]BF4

: 910327-76-3,483306-17-8
W₂Cp₂(μ-PPh₂)₂(CO)₂

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; (N2); 1,8-diazabicyclo(5.4.0)undec-7-ene added to a soln. of W complex;
DOI:10.1021/ic060544n