(C₆H₅)2P(CH₂)2P(C₆H₅)2(AuNO₃)2

Base Information

• Chemical Name: (C₆H₅)2P(CH₂)2P(C₆H₅)2(AuNO₃)2
• CAS No.: 119688-08-3
• Molecular Formula: C₂₆H₂₄Au₂N₂O₆P₂
• Molecular Weight: 916.367

Synonyms:

Chemical Property of (C₆H₅)2P(CH₂)2P(C₆H₅)2(AuNO₃)2

Chemical Property:

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Technology Process of (C₆H₅)2P(CH₂)2P(C₆H₅)2(AuNO₃)2

There total 1 articles about (C₆H₅)2P(CH₂)2P(C₆H₅)2(AuNO₃)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

1,2-bis(diphenylphosphino)ethane digold(I) dichloride (18024-34-5) + silver nitrate → (C6H5)2P(CH2)2P(C6H5)2(AuNO3)2 (119688-08-3)

Guidance literature:

In further solvent(s); byproducts: AgCl; under N2, addn. of AgNO3 in a minimum amount of EtOH/water to a stirred soln. of Au-complex in CH2Cl2, stirring mixt. at ambient temp. for 30 min, shielded from light, filtration through diatomaceous earth, pptn. by addn. of diethyl ether; dissolved in CH2Cl2, again pptd. with diethyl ether; elem. anal.;

DOI:10.1016/S0020-1693(00)89278-6

Reference yield: 89.0%

(C6H5)2P(CH2)2P(C6H5)2(AuNO3)2 (119688-08-3) + ammonia (7664-41-7) → 1,2-bis(diphenylphosphino)ethanebis(amminegold(I))nitrate

Guidance literature:

In dichloromethane; under N2, Au-complex dissolved in CH2Cl2, filtered through diatomaceous earth, gaseous NH3 slowly passed through filtrate for 2h,N2 passed through soln., white pptn.; filtration, washed with diethyl ether, dried in air; elem. anal.;

DOI:10.1016/S0020-1693(00)89278-6

Reference yield: 76.0%

propylamine (107-10-8,42939-71-9) + (C6H5)2P(CH2)2P(C6H5)2(AuNO3)2 (119688-08-3) → (AuNH2CH2CH2CH3)2(P(C6H5)2(CH2)2P(C6H5)2)(2+)*2NO3(1-)={(AuNH2CH2CH2CH3)2(P(C6H5)2(CH2)2P(C6H5)2)}(NO3)2

Guidance literature:

In dichloromethane; under N2, Au-complex dissolved in CH2Cl2, filtered through diatomaceous earth, addn. of amine to the stirred filtrate via syringe, soln. concd. under a stream of N2, ppt.; filtration, washed (diethyl ether), dried in air; elem. anal.;

DOI:10.1016/S0020-1693(00)89278-6

upstream raw materials:

1,2-bis(diphenylphosphino)ethane digold(I) dichloride

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