Technology Process of cis-1-benzyl-1,2,3,4,4a,5,11,11a-octahydro-6H-pyrido<3,2-b>carbazole
There total 6 articles about cis-1-benzyl-1,2,3,4,4a,5,11,11a-octahydro-6H-pyrido<3,2-b>carbazole which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
for 16h;
Heating;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 51.6 percent / H2 / 5percent Rh/Al2O3 / ethanol / 10 h / 100 °C / 41371.8 Torr
2: 77.2 percent / K2CO3 / benzene / 24 h / 37 °C
3: 42.8 percent / CrO3, H2SO4 / 1.) 0-2 deg C, 30 min, 2.) 25-30 deg C, 1 h
4: 24.65 percent / concd. HCl / ethanol / 4 h / Heating
5: 84 percent / LiAlH4 / tetrahydrofuran / 16 h / Heating
With
chromium(VI) oxide; hydrogenchloride; lithium aluminium tetrahydride; sulfuric acid; hydrogen; potassium carbonate;
Rh/Al2O3;
In
tetrahydrofuran; ethanol; benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 77.2 percent / K2CO3 / benzene / 24 h / 37 °C
2: 42.8 percent / CrO3, H2SO4 / 1.) 0-2 deg C, 30 min, 2.) 25-30 deg C, 1 h
3: 24.65 percent / concd. HCl / ethanol / 4 h / Heating
4: 84 percent / LiAlH4 / tetrahydrofuran / 16 h / Heating
With
chromium(VI) oxide; hydrogenchloride; lithium aluminium tetrahydride; sulfuric acid; potassium carbonate;
In
tetrahydrofuran; ethanol; benzene;
