(R)-2-{(4R,5R,6R)-6-[(R)-2-(tert-Butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-3-oxo-3-(2-oxo-oxazolidin-3-yl)-propionaldehyde

Base Information

Chemical Name:(R)-2-{(4R,5R,6R)-6-[(R)-2-(tert-Butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-3-oxo-3-(2-oxo-oxazolidin-3-yl)-propionaldehyde
CAS No.:121425-40-9
Molecular Formula:C₃₂H₄₃NO₇Si
Molecular Weight:581.781
Hs Code.:

(R)-2-{(4R,5R,6R)-6-[(R)-2-(tert-Butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-3-oxo-3-(2-oxo-oxazolidin-3-yl)-propionaldehyde

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Chemical Property of (R)-2-{(4R,5R,6R)-6-[(R)-2-(tert-Butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-3-oxo-3-(2-oxo-oxazolidin-3-yl)-propionaldehyde

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Technology Process of (R)-2-{(4R,5R,6R)-6-[(R)-2-(tert-Butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-3-oxo-3-(2-oxo-oxazolidin-3-yl)-propionaldehyde

There total 4 articles about (R)-2-{(4R,5R,6R)-6-[(R)-2-(tert-Butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-3-oxo-3-(2-oxo-oxazolidin-3-yl)-propionaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106568-13-2,121440-66-2
(2R,3R,4R)-5-((tert-butyldiphenylsilyl)oxy)-2,4-dimethyl-3-((triethylsilyl)oxy)pentanal

: 121425-40-9
(R)-2-{(4R,5R,6R)-6-[(R)-2-(tert-Butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-3-oxo-3-(2-oxo-oxazolidin-3-yl)-propionaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Bu₂BOTf, Et₃N, 2.) H₂O₂ / 1.) CH₂Cl₂, from -78 deg C to -50 deg C, 2.) pH 7

2: pTsOH, H₂O / tetrahydrofuran

3: pTsOH

4: 1.) O₃, 2.) Me₂S / 1.) MeOH, -78 deg C

With dimethylsulfide; di-n-butylboryl trifluoromethanesulfonate; water; dihydrogen peroxide; toluene-4-sulfonic acid; ozone; triethylamine; In tetrahydrofuran;
DOI:10.1021/jo00274a008

Reference yield:

: 121440-67-3
3-[(2S,3R,4S,5R,6R)-7-(tert-Butyl-diphenyl-silanyloxy)-3-hydroxy-4,6-dimethyl-5-triethylsilanyloxy-2-vinyl-heptanoyl]-oxazolidin-2-one

: 121425-40-9
(R)-2-{(4R,5R,6R)-6-[(R)-2-(tert-Butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-3-oxo-3-(2-oxo-oxazolidin-3-yl)-propionaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: pTsOH, H₂O / tetrahydrofuran

2: pTsOH

3: 1.) O₃, 2.) Me₂S / 1.) MeOH, -78 deg C

With dimethylsulfide; water; toluene-4-sulfonic acid; ozone; In tetrahydrofuran;
DOI:10.1021/jo00274a008

Reference yield:

: 109299-92-5
3-((E)-but-2-enoyl)oxazolidin-2-one

: 121425-40-9
(R)-2-{(4R,5R,6R)-6-[(R)-2-(tert-Butyl-diphenyl-silanyloxy)-1-methyl-ethyl]-2,2,5-trimethyl-[1,3]dioxan-4-yl}-3-oxo-3-(2-oxo-oxazolidin-3-yl)-propionaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Bu₂BOTf, Et₃N, 2.) H₂O₂ / 1.) CH₂Cl₂, from -78 deg C to -50 deg C, 2.) pH 7

2: pTsOH, H₂O / tetrahydrofuran

3: pTsOH

4: 1.) O₃, 2.) Me₂S / 1.) MeOH, -78 deg C

With dimethylsulfide; di-n-butylboryl trifluoromethanesulfonate; water; dihydrogen peroxide; toluene-4-sulfonic acid; ozone; triethylamine; In tetrahydrofuran;
DOI:10.1021/jo00274a008