N4-(4-methoxybenzyl)-2-chloropyridine-3,4-diamine

Base Information

Chemical Name:N4-(4-methoxybenzyl)-2-chloropyridine-3,4-diamine
CAS No.:881844-10-6
Molecular Formula:C13H14ClN3O
Molecular Weight:263.727
Hs Code.:
Mol file:881844-10-6.mol

Synonyms:3-amino-2-chloro-4-(p-methoxybenzylamino)pyridine;3,4-Pyridinediamine,2-chloro-N4-[(4-methoxyphenyl)methyl];N4-(4-methoxybenzyl)-2-chloropyridine-3,4-diamine;2-chloro-N4-(4-methoxybenzyl)pyridine-3,4-diamine;

Suppliers and Price of N4-(4-methoxybenzyl)-2-chloropyridine-3,4-diamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-Chloro-N4-(4-methoxybenzyl)pyridine-3,4-diamine 95+%
1g
$ 510.00

Chemenu
2-chloro-N4-(4-methoxybenzyl)pyridine-3,4-diamine 95%
1g
$ 482.00

Chemcia Scientific
2-Chloro-N*4*-(4-methoxy-benzyl)-pyridine-3,4-diamine 95%
1 G
$ 495.00

Chemcia Scientific
2-Chloro-N*4*-(4-methoxy-benzyl)-pyridine-3,4-diamine 95%
0.5 G
$ 330.00

American Custom Chemicals Corporation
2-CHLORO-N4-(4-METHOXYBENZYL)PYRIDINE-3,4-DIAMINE 95.00%
5MG
$ 500.86

Total 16 raw suppliers

Chemical Property of N4-(4-methoxybenzyl)-2-chloropyridine-3,4-diamine

Chemical Property:

PSA：60.17000
LogP:3.59210
Storage Temp.:2-8°C

Purity/Quality:

99% ^*data from raw suppliers

2-Chloro-N4-(4-methoxybenzyl)pyridine-3,4-diamine 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N4-(4-methoxybenzyl)-2-chloropyridine-3,4-diamine

There total 5 articles about N4-(4-methoxybenzyl)-2-chloropyridine-3,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 881844-09-3
2-chloro-N-(4-methoxybenzyl)-3-nitropyridin-4-amine

: 881844-10-6
2-chloro-N⁴-(4-methoxybenzyl)pyridine-3,4-diamine

Guidance literature:: With iron; ammonium chloride; In ethanol; water; for 6h; Reflux;
DOI:10.1021/acs.jmedchem.0c01411

Reference yield: 60.0%

: 881844-09-3
2-chloro-N-(4-methoxybenzyl)-3-nitropyridin-4-amine

: 7439-89-6
iron

: 881844-10-6
2-chloro-N⁴-(4-methoxybenzyl)pyridine-3,4-diamine

Guidance literature:: With hydrogenchloride; In methanol; water;

Reference yield:

: 5975-12-2
2,4-dichloro-3-nitro-pyridine

: 881844-10-6
2-chloro-N⁴-(4-methoxybenzyl)pyridine-3,4-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: 33 g / triethylamine / dimethylformamide / 2 h / 20 °C

2: 28.6 g / H₂; Raney Ni / methanol / 3.5 h / 20 °C

With hydrogen; nickel; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.10.040