C₂₆H₂₈ClN₅O₄S₂*ClH

Base Information

Chemical Name:C₂₆H₂₈ClN₅O₄S₂*ClH
CAS No.:1425941-51-0
Molecular Formula:C₂₆H₂₈ClN₅O₄S₂*ClH
Molecular Weight:610.585
Hs Code.:

C<sub>26</sub>H<sub>28</sub>ClN<sub>5</sub>O<sub>4</sub>S<sub>2</sub>*ClH

Synonyms:

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Chemical Property of C₂₆H₂₈ClN₅O₄S₂*ClH

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Technology Process of C₂₆H₂₈ClN₅O₄S₂*ClH

There total 6 articles about C₂₆H₂₈ClN₅O₄S₂*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 886362-07-8
4-(methyloxy)-1H-indazol-3-amine

: 1425941-51-0
C₂₆H₂₈ClN₅O₄S₂*ClH

Guidance literature:: Multi-step reaction with 5 steps

1: potassium hydroxide / dimethyl sulfoxide / 0.42 h / 20 °C / Inert atmosphere

2: pyridine / 0.67 h / 20 °C / Inert atmosphere

3: lithium aluminium tetrahydride; hydrogenchloride / diethyl ether; tetrahydrofuran / 1 h / 10 - 20 °C / Inert atmosphere

4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-methyl-morpholine / N,N-dimethyl-formamide

5: dichloromethane / Acidic conditions

With 4-methyl-morpholine; pyridine; hydrogenchloride; lithium aluminium tetrahydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; potassium hydroxide; In tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm301572h

Reference yield:

: 1240518-02-8
3-{[3-amino-4-(methyloxy)-1H-indazol-1-yl]methyl}-benzonitrile

: 1425941-51-0
C₂₆H₂₈ClN₅O₄S₂*ClH

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 0.67 h / 20 °C / Inert atmosphere

2: lithium aluminium tetrahydride; hydrogenchloride / diethyl ether; tetrahydrofuran / 1 h / 10 - 20 °C / Inert atmosphere

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-methyl-morpholine / N,N-dimethyl-formamide

4: dichloromethane / Acidic conditions

With 4-methyl-morpholine; pyridine; hydrogenchloride; lithium aluminium tetrahydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm301572h

Reference yield:

: 1240518-03-9
5-chloro-N-{1-[(3-cyanophenyl)methyl]-4-(methoxy)-1H-indazole-3-yl}-2-thiophene sulphonamide

: 1425941-51-0
C₂₆H₂₈ClN₅O₄S₂*ClH

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride; hydrogenchloride / diethyl ether; tetrahydrofuran / 1 h / 10 - 20 °C / Inert atmosphere

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-methyl-morpholine / N,N-dimethyl-formamide

3: dichloromethane / Acidic conditions

With 4-methyl-morpholine; hydrogenchloride; lithium aluminium tetrahydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm301572h