[Ru(4,7-diphenyl-1,10-phenanthroline)(SCN)2(4-(6-oxo-[1,10]phenanthroline-5-ylideneamino)-3-hydroxynaphthalene-1-sulfonic acid)]

Base Information

• Chemical Name: [Ru(4,7-diphenyl-1,10-phenanthroline)(SCN)2(4-(6-oxo-[1,10]phenanthroline-5-ylideneamino)-3-hydroxynaphthalene-1-sulfonic acid)]
• CAS No.: 1612890-70-6
• Molecular Formula: C₄₈H₂₉N₇O₅RuS₃
• Molecular Weight: 981.07
• Mol file: 1612890-70-6.mol

Synonyms:

Chemical Property of [Ru(4,7-diphenyl-1,10-phenanthroline)(SCN)2(4-(6-oxo-[1,10]phenanthroline-5-ylideneamino)-3-hydroxynaphthalene-1-sulfonic acid)]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Ru(4,7-diphenyl-1,10-phenanthroline)(SCN)2(4-(6-oxo-[1,10]phenanthroline-5-ylideneamino)-3-hydroxynaphthalene-1-sulfonic acid)]

There total 3 articles about [Ru(4,7-diphenyl-1,10-phenanthroline)(SCN)2(4-(6-oxo-[1,10]phenanthroline-5-ylideneamino)-3-hydroxynaphthalene-1-sulfonic acid)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

bathophenanthroline (1662-01-7) + [RuCl2(ethanol)2(4-(6-oxo-[1,10]phenanthroline-5-ylideneamino)-3-hydroxynaphthalene-1-sulfonic acid)] + potassium thioacyanate (333-20-0) → [Ru(4,7-diphenyl-1,10-phenanthroline)(SCN)2(4-(6-oxo-[1,10]phenanthroline-5-ylideneamino)-3-hydroxynaphthalene-1-sulfonic acid)] (1612890-70-6)

Guidance literature:

In ethanol; for 4h; Inert atmosphere; Reflux;

DOI:10.1039/c3dt52949e

Reference yield:

1,10-Phenanthroline (66-71-7) → [Ru(4,7-diphenyl-1,10-phenanthroline)(SCN)2(4-(6-oxo-[1,10]phenanthroline-5-ylideneamino)-3-hydroxynaphthalene-1-sulfonic acid)] (1612890-70-6)

Guidance literature:

Multi-step reaction with 4 steps

1: potassium bromide; sulfuric acid; nitric acid / 4 h / Reflux

2: ethanol / 4 h / Reflux

3: 4 h / Inert atmosphere; Reflux

4: ethanol / 4 h / Inert atmosphere; Reflux

With sulfuric acid; nitric acid; potassium bromide; In ethanol;

DOI:10.1039/c3dt52949e

Reference yield:

1,10-phenanthroline-5,6-dione (27318-90-7) → [Ru(4,7-diphenyl-1,10-phenanthroline)(SCN)2(4-(6-oxo-[1,10]phenanthroline-5-ylideneamino)-3-hydroxynaphthalene-1-sulfonic acid)] (1612890-70-6)

Guidance literature:

Multi-step reaction with 3 steps

1: ethanol / 4 h / Reflux

2: 4 h / Inert atmosphere; Reflux

3: ethanol / 4 h / Inert atmosphere; Reflux

In ethanol;

DOI:10.1039/c3dt52949e

upstream raw materials:

bathophenanthroline

potassium thioacyanate

1,10-Phenanthroline

1,10-phenanthroline-5,6-dione