2-((E)-9-Phenylsulfanylmethyl-deca-5,9-dienyloxy)-tetrahydro-pyran

Base Information

Chemical Name:2-((E)-9-Phenylsulfanylmethyl-deca-5,9-dienyloxy)-tetrahydro-pyran
CAS No.:141502-92-3
Molecular Formula:C₂₂H₃₂O₂S
Molecular Weight:360.561
Hs Code.:

Synonyms:

Suppliers and Price of 2-((E)-9-Phenylsulfanylmethyl-deca-5,9-dienyloxy)-tetrahydro-pyran

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-((E)-9-Phenylsulfanylmethyl-deca-5,9-dienyloxy)-tetrahydro-pyran

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-((E)-9-Phenylsulfanylmethyl-deca-5,9-dienyloxy)-tetrahydro-pyran

There total 11 articles about 2-((E)-9-Phenylsulfanylmethyl-deca-5,9-dienyloxy)-tetrahydro-pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 141502-83-2
4-Methoxymethoxymethyl-pent-4-enal

: 141502-92-3
2-((E)-9-Phenylsulfanylmethyl-deca-5,9-dienyloxy)-tetrahydro-pyran

Guidance literature:: Multi-step reaction with 9 steps

1: 82 percent / NaH

2: 88 percent / p-TsOH / ethanol

3: 85 percent

4: 95 percent / DIBAL

5: 64 percent / LiBr, MsCl, Et₃N

6: 57 percent / LDA

7: Na-Hg / ethanol

8: n-Bu₃NF

9: n-Bu₃P

With sodium amalgam; tributylphosphine; n-Bu₃NF; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; methanesulfonyl chloride; triethylamine; lithium bromide; lithium diisopropyl amide; In ethanol;
DOI:10.1246/cl.1992.527

Reference yield:

: 141502-82-1
4-Methoxymethoxymethyl-pent-4-en-1-ol

: 141502-92-3
2-((E)-9-Phenylsulfanylmethyl-deca-5,9-dienyloxy)-tetrahydro-pyran

Guidance literature:: Multi-step reaction with 10 steps

1: 84 percent / (COCl)2, DMSO

2: 82 percent / NaH

3: 88 percent / p-TsOH / ethanol

4: 85 percent

5: 95 percent / DIBAL

6: 64 percent / LiBr, MsCl, Et₃N

7: 57 percent / LDA

8: Na-Hg / ethanol

9: n-Bu₃NF

10: n-Bu₃P

With sodium amalgam; oxalyl dichloride; tributylphosphine; n-Bu₃NF; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; methanesulfonyl chloride; triethylamine; lithium bromide; lithium diisopropyl amide; In ethanol;
DOI:10.1246/cl.1992.527

Reference yield:

: 141502-81-0
4-Methoxymethoxymethyl-pent-4-enoic acid methyl ester

: 141502-92-3
2-((E)-9-Phenylsulfanylmethyl-deca-5,9-dienyloxy)-tetrahydro-pyran

Guidance literature:: Multi-step reaction with 11 steps

1: 95 percent / LiAlH₄

2: 84 percent / (COCl)2, DMSO

3: 82 percent / NaH

4: 88 percent / p-TsOH / ethanol

5: 85 percent

6: 95 percent / DIBAL

7: 64 percent / LiBr, MsCl, Et₃N

8: 57 percent / LDA

9: Na-Hg / ethanol

10: n-Bu₃NF

11: n-Bu₃P

With lithium aluminium tetrahydride; sodium amalgam; oxalyl dichloride; tributylphosphine; n-Bu₃NF; sodium hydride; diisobutylaluminium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; methanesulfonyl chloride; triethylamine; lithium bromide; lithium diisopropyl amide; In ethanol;
DOI:10.1246/cl.1992.527