((C₅H₅)V(C₆H₅)P(C₆H₅)2)

Base Information

Chemical Name:((C₅H₅)V(C₆H₅)P(C₆H₅)2)
CAS No.:89184-67-8
Molecular Formula:C₂₃H₂₀PV
Molecular Weight:378.327
Hs Code.:

((C<sub>5</sub>H<sub>5</sub>)V(C<sub>6</sub>H<sub>5</sub>)P(C<sub>6</sub>H<sub>5</sub>)2)

Synonyms:

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Chemical Property of ((C₅H₅)V(C₆H₅)P(C₆H₅)2)

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Technology Process of ((C₅H₅)V(C₆H₅)P(C₆H₅)2)

There total 1 articles about ((C₅H₅)V(C₆H₅)P(C₆H₅)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: K⁽¹⁺⁾*1.5C₄H₈O*((C₅H₅)V(C₆H₅)P(C₆H₅)2)^(1-)=(K(C₄H₈O)1.5)((C₅H₅)V(C₆H₅)P(C₆H₅)2)

: ZnCl₂*1.5C₄H₈O

: 89184-67-8
((C₅H₅)V(C₆H₅)P(C₆H₅)2)

Guidance literature:: In tetrahydrofuran; addn. of a soln. of ZnCl2*1.5THF in THF to a soln. of CpV(C6H5)P(C6H5)2in THF at room temp. (Ar) and stirring for 30 min; concn. of the filtrate, addn. of ether and cooling to -78°C, pptn. of sand-yellow crystals, filtering off the crystals, washing with ether and drying (oil pump vacuum), elem. anal.;

Reference yield: 65.0%

: 89184-67-8
((C₅H₅)V(C₆H₅)P(C₆H₅)2)

: 201230-82-2
carbon monoxide

: 12213-09-1
tricarbonyl(η-cyclopentadienyl)triphenylphosphinevanadium

Guidance literature:: In tetrahydrofuran; reaction of CpV(C6H5)P(C6H5)2 with CO at room temp. (Ar); evapn. of the reaction soln. to dryness and dissolving the residue in toluene, pptn. of red brown crystals on cooling to -78°C, filtering off the crystals and drying (oil pump vacuum), elem. anal.;

Reference yield: 58.0%

: 89184-67-8
((C₅H₅)V(C₆H₅)P(C₆H₅)2)

: 106-95-6
allyl bromide

: 89184-54-3
(ηcyclopentadienyl)(η3-allyl)(triphenylphosphane)vanadium

Guidance literature:: In tetrahydrofuran; addn. of allyl bromide to a soln. of CpV(C6H5)P(C6H5)2 in THF at room temp. (Ar); concn. of the soln. and addn. of ether, formation of a red ppt., filtering off the ppt., washing with ether and drying (oil pump vacuum), elem.anal.;