Technology Process of C22H21ClN2O6S
There total 6 articles about C22H21ClN2O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dimethylformamide / 1 h / 100 °C
2: 1.) potassium tert-butoxide / 1.) THF, 60 deg C, 45 min, 2.) THF, reflux, 3 h
3: acetic anhydride / 0.83 h / Heating
4: dimethylsulfoxide / 1.42 h / Ambient temperature
5: 1.) hydrogen chloride / 1.) RT, 5 d, 2.) reflux, 4 h
With
hydrogenchloride; potassium tert-butylate; acetic anhydride;
In
dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm00102a016
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dimethylformamide / 1 h / 100 °C
2: 1.) potassium tert-butoxide / 1.) THF, 60 deg C, 45 min, 2.) THF, reflux, 3 h
3: acetic anhydride / 0.83 h / Heating
4: dimethylsulfoxide / 1.42 h / Ambient temperature
5: 1.) hydrogen chloride / 1.) RT, 5 d, 2.) reflux, 4 h
With
hydrogenchloride; potassium tert-butylate; acetic anhydride;
In
dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jm00102a016
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) potassium tert-butoxide / 1.) THF, 60 deg C, 45 min, 2.) THF, reflux, 3 h
2: acetic anhydride / 0.83 h / Heating
3: dimethylsulfoxide / 1.42 h / Ambient temperature
4: 1.) hydrogen chloride / 1.) RT, 5 d, 2.) reflux, 4 h
With
hydrogenchloride; potassium tert-butylate; acetic anhydride;
In
dimethyl sulfoxide;
DOI:10.1021/jm00102a016
