Benzeneacetic acid, 3-[4-[[[2-(2,4-dichlorophenoxy)ethyl]amino]carbonyl

Base Information

Chemical Name:Benzeneacetic acid, 3-[4-[[[2-(2,4-dichlorophenoxy)ethyl]amino]carbonyl
CAS No.:870194-96-0
Molecular Formula:C₂₆H₂₀Cl₂N₂O₅
Molecular Weight:511.361
Hs Code.:
Mol file:870194-96-0.mol

Synonyms:HINPKGVWVQYESB-UHFFFAOYSA-N;Benzeneacetic acid, 3-[4-[[[2-(2,4-dichlorophenoxy)ethyl]aMino]carbonyl;Benzeneacetic acid, 3-[4-[[[2-(2,4-dichlorophenoxy)ethyl]amino]carbonyl]-5-phenyl-3-isoxazolyl]-

Suppliers and Price of Benzeneacetic acid, 3-[4-[[[2-(2,4-dichlorophenoxy)ethyl]amino]carbonyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
3-[4-[[[2-(2,4-DICHLOROPHENOXY)ETHYL]AMINO]CARBONYL]-5-PHENYL-3-ISOXAZOLYL]BENZENEACETIC ACID 95.00%
5MG
$ 505.46

Total 2 raw suppliers

Chemical Property of Benzeneacetic acid, 3-[4-[[[2-(2,4-dichlorophenoxy)ethyl]amino]carbonyl

Chemical Property:

PSA：105.15000
LogP:6.32610

Purity/Quality:

99% ^*data from raw suppliers

3-[4-[[[2-(2,4-DICHLOROPHENOXY)ETHYL]AMINO]CARBONYL]-5-PHENYL-3-ISOXAZOLYL]BENZENEACETIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzeneacetic acid, 3-[4-[[[2-(2,4-dichlorophenoxy)ethyl]amino]carbonyl

There total 17 articles about Benzeneacetic acid, 3-[4-[[[2-(2,4-dichlorophenoxy)ethyl]amino]carbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42058-59-3
3-hydroxy-benzeneacetic acid, methyl ester

: 870194-96-0
LC₁₇₆₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: NEt₃ / CH₂Cl₂ / 1 h / 0 °C

2.1: Pd(PPh₃)4 / dimethylformamide / 30 h / 80 °C

3.1: formic acid / Raney-nickel / 10 h / 110 °C

4.1: H₂NOH*HCl; aq. Na₂CO₃ / 2 h / 20 °C

5.1: NCS; HCl(gas) / dimethylformamide / 0.5 h / 20 °C

6.1: potassium bis(trimethylsilyl)amide / diethyl ether / 1 h / 20 °C

6.2: acetonitrile / 3 h / 20 °C

7.1: aq. LiOH / tetrahydrofuran / 12 h / 20 °C

With hydrogenchloride; lithium hydroxide; N-chloro-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; formic acid; hydroxylamine hydrochloride; potassium hexamethylsilazane; sodium carbonate; triethylamine; nickel; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2006.08.052

Reference yield:

: 927187-47-1
(3-{4-[2-(2,4-dichloro-phenoxy)-ethyl-carbamoyl]-5-phenyl-isoxazol-3-yl}-phenyl)-acetic acid methyl ester

: 870194-96-0
LC₁₇₆₅

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1016/j.bmcl.2006.08.052

Reference yield:

: 52798-00-2
(3-cyano-phenyl)-acetic acid methyl ester

: 870194-96-0
LC₁₇₆₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: formic acid / Raney-nickel / 10 h / 110 °C

2.1: H₂NOH*HCl; aq. Na₂CO₃ / 2 h / 20 °C

3.1: NCS; HCl(gas) / dimethylformamide / 0.5 h / 20 °C

4.1: potassium bis(trimethylsilyl)amide / diethyl ether / 1 h / 20 °C

4.2: acetonitrile / 3 h / 20 °C

5.1: aq. LiOH / tetrahydrofuran / 12 h / 20 °C

With hydrogenchloride; lithium hydroxide; N-chloro-succinimide; formic acid; hydroxylamine hydrochloride; potassium hexamethylsilazane; sodium carbonate; nickel; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2006.08.052