C₂₇H₂₃FO₈

Base Information

• Chemical Name: C₂₇H₂₃FO₈
• CAS No.: 1228019-05-3
• Molecular Formula: C₂₇H₂₃FO₈
• Molecular Weight: 494.473
• Mol file: 1228019-05-3.mol

Synonyms:

Chemical Property of C₂₇H₂₃FO₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₇H₂₃FO₈

There total 5 articles about C₂₇H₂₃FO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-deoxy-4-fluoro-1-O-acetyl-2,3,6-tri-O-benzoyl-D-glucopyranose (701936-21-2) → C27H23FO8 + C27H23FO8 (1228019-05-3)

Guidance literature:

With acetic acid; ethylenediamine; In tetrahydrofuran; at 0 - 20 ℃; Large scale reaction;

DOI:10.1021/op100053k

Reference yield:

benzoyl chloride (98-88-4) → C27H23FO8 + C27H23FO8 (1228019-05-3)

Guidance literature:

Multi-step reaction with 4 steps

1: pyridine / 9 - 18 °C / Large scale reaction

2: (bis-(2-methoxyethyl)amino)sulfur trufluoride / tetrahydrofuran / 20 - 52 °C / Large scale reaction

3: sulfuric acid / 1 h / 50 °C / Large scale reaction

4: acetic acid; ethylenediamine / tetrahydrofuran / 0 - 20 °C / Large scale reaction

With pyridine; sulfuric acid; acetic acid; ethylenediamine; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In tetrahydrofuran;

DOI:10.1021/op100053k

Reference yield:

Methyl 2,3,6-Tri-O-benzoyl-4-deoxy-4-fluoro-α-D-glucopyranoside (84065-98-5) → C27H23FO8 + C27H23FO8 (1228019-05-3)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid / 1 h / 50 °C / Large scale reaction

2: acetic acid; ethylenediamine / tetrahydrofuran / 0 - 20 °C / Large scale reaction

With sulfuric acid; acetic acid; ethylenediamine; In tetrahydrofuran;

DOI:10.1021/op100053k

upstream raw materials:

methyl 2,3,6-tri-O-benzoyl-α-D-galactopyranoside

4-deoxy-4-fluoro-1-O-acetyl-2,3,6-tri-O-benzoyl-D-glucopyranose

benzoyl chloride

Methyl 2,3,6-Tri-O-benzoyl-4-deoxy-4-fluoro-α-D-glucopyranoside