hexadecanedioic acid monoethyl ester

Base Information

• Chemical Name: hexadecanedioic acid monoethyl ester
• CAS No.: 18017-66-8
• Molecular Formula: C₁₈H₃₄O₄
• Molecular Weight: 314.466
• Mol file: 18017-66-8.mol

Synonyms:

Chemical Property of hexadecanedioic acid monoethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of hexadecanedioic acid monoethyl ester

There total 1 articles about hexadecanedioic acid monoethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

ethanol (64-17-5) + thapsic acid (505-54-4) → diethyl hexadecanedioate (15786-31-9) + hexadecanedioic acid monoethyl ester (18017-66-8)

Guidance literature:

With sulfuric acid; In cyclohexane; for 48h;

DOI:10.1021/ja00228a032

Reference yield:

hexadecanedioic acid monoethyl ester (18017-66-8) → 15-aminopentadecanoic acid (17437-21-7)

Guidance literature:

Multi-step reaction with 4 steps

1: thionyl chloride

2: benzene; ammonia

3: water; bromine

4: concentrated aqueous HCl

With hydrogenchloride; thionyl chloride; ammonia; water; bromine; benzene;

DOI:10.1021/ja01539a058

upstream raw materials:

ethanol

thapsic acid

Downstream raw materials:

15-aminopentadecanoic acid

Refernces