triphenyl(pyrocatecholato-O,O)antimony(V) dimethyl sulfoxide adduct

Base Information

• Chemical Name: triphenyl(pyrocatecholato-O,O)antimony(V) dimethyl sulfoxide adduct
• CAS No.: 256495-78-0
• Molecular Formula: C₆H₆*C₂₆H₂₅O₃SSb
• Molecular Weight: 617.412
• Mol file: 256495-78-0.mol

Synonyms:

Chemical Property of triphenyl(pyrocatecholato-O,O)antimony(V) dimethyl sulfoxide adduct

Chemical Property:

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Technology Process of triphenyl(pyrocatecholato-O,O)antimony(V) dimethyl sulfoxide adduct

There total 1 articles about triphenyl(pyrocatecholato-O,O)antimony(V) dimethyl sulfoxide adduct which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

triphenylantimony (603-36-1) + benzene-1,2-diol (120-80-9,19481-10-8,37349-32-9) + dimethyl sulfoxide (67-68-5,8070-53-9) → triphenyl(pyrocatecholato-O,O)antimony(V) dimethyl sulfoxide adduct (256495-78-0)

Guidance literature:

With (CH₃)3COOH; In benzene; soln. of t-Bu-hydroperoxide addn. to mixture of Sb-compd., diphenol, andDMSO in benzene, volatile products condensing under reduced pressure; recrystn (benzene-hexane); elem. anal.;

DOI:10.1007/BF02494820

upstream raw materials:

triphenylantimony

benzene-1,2-diol

dimethyl sulfoxide