Phenyl 6-ethyl-3-(N-methoxy-N-methylcarbomoyl)-1,2-dihydropyridinecarboxylate

Base Information

Chemical Name:Phenyl 6-ethyl-3-(N-methoxy-N-methylcarbomoyl)-1,2-dihydropyridinecarboxylate
CAS No.:389570-71-2
Molecular Formula:C₁₇H₂₀N₂O₄
Molecular Weight:316.357
Hs Code.:

Synonyms:

Suppliers and Price of Phenyl 6-ethyl-3-(N-methoxy-N-methylcarbomoyl)-1,2-dihydropyridinecarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Phenyl 6-ethyl-3-(N-methoxy-N-methylcarbomoyl)-1,2-dihydropyridinecarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Phenyl 6-ethyl-3-(N-methoxy-N-methylcarbomoyl)-1,2-dihydropyridinecarboxylate

There total 2 articles about Phenyl 6-ethyl-3-(N-methoxy-N-methylcarbomoyl)-1,2-dihydropyridinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 925-90-6
ethylmagnesium bromide

: 95091-91-1
N-methoxy-N-methylpyridine-3-carboxamide

: 1885-14-9
phenyl chloroformate

: Phenyl 4-ethyl-3-(N-methoxy-N-methylcarbamoyl)-1,4-dihydropyridinecarboxylate

: 389570-71-2
Phenyl 6-ethyl-3-(N-methoxy-N-methylcarbomoyl)-1,2-dihydropyridinecarboxylate

: Phenyl 2-ethyl-3-(N-methoxy-N-methylcarbamoyl)-1,4-dihydropyridinecarboxylate

Guidance literature:: N-methoxy-N-methylpyridine-3-carboxamide; phenyl chloroformate; With copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; at -78 ℃; for 0.333333h;

ethylmagnesium bromide; In tetrahydrofuran; for 1h;
DOI:10.1055/s-2001-17509

Reference yield:

: 59-67-6
nicotinic acid

: 389570-71-2
Phenyl 6-ethyl-3-(N-methoxy-N-methylcarbomoyl)-1,2-dihydropyridinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 95 percent / HOBt*H₂O; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide*HCl; Et₃N / acetonitrile / 2 h / 20 °C

2.1: CuBr*Me₂S / tetrahydrofuran / 0.33 h / -78 °C

2.2: tetrahydrofuran / 1 h

With copper(I) bromide dimethylsulfide complex; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; acetonitrile;
DOI:10.1055/s-2001-17509