Benzoic acid, 5-chloro-2-methoxy-4-methyl-3-nitro-, methyl ester

Base Information

Chemical Name:Benzoic acid, 5-chloro-2-methoxy-4-methyl-3-nitro-, methyl ester
CAS No.:907190-25-4
Molecular Formula:C10H10ClNO5
Molecular Weight:259.646
Hs Code.:

Synonyms:methyl 5-chloro-2-methoxy-4-methyl-3-nitrobenzoate;Benzoic acid, 5-chloro-2-methoxy-4-methyl-3-nitro-, methyl ester

Suppliers and Price of Benzoic acid, 5-chloro-2-methoxy-4-methyl-3-nitro-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 4 raw suppliers

Chemical Property of Benzoic acid, 5-chloro-2-methoxy-4-methyl-3-nitro-, methyl ester

Chemical Property:

Boiling Point:382.2±37.0 °C(Predicted)
PSA：81.35000
Density:1.356±0.06 g/cm3(Predicted)
LogP:2.87500

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 5-chloro-2-methoxy-4-methyl-3-nitro-, methyl ester

There total 2 articles about Benzoic acid, 5-chloro-2-methoxy-4-methyl-3-nitro-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 907190-23-2
5-chloro-2-methoxy-4-methyl-benzoic acid methyl ester

: 907190-25-4
5-chloro-2-methoxy-4-methyl-3-nitrobenzoic acid methyl ester

Guidance literature:: With nitric acid; acetic anhydride; acetic acid; at 20 ℃; for 18h;
DOI:10.1021/jm060408s

Reference yield:

: 81245-24-1
methyl 4-methyl-2-methoxybenzoate

: 907190-25-4
5-chloro-2-methoxy-4-methyl-3-nitrobenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NCS / dimethylformamide / 72 h / 20 °C

2: 18.45 g / HNO₃; AcOH; Ac₂O / 18 h / 20 °C

With N-chloro-succinimide; nitric acid; acetic anhydride; acetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jm060408s

Reference yield: 98.0%

: 907190-25-4
5-chloro-2-methoxy-4-methyl-3-nitrobenzoic acid methyl ester

: 907190-26-5
3-amino-2-methoxy-4-methylbenzoic acid methyl ester

Guidance literature:: With hydrogen; triethylamine; palladium dihydroxide; In ethanol; at 20 ℃; for 8h; under 2585.74 Torr;
DOI:10.1021/jm060408s