MoI(CO)3P(C₆H₅)2(CH₂)3P(C₆H₅)2NCCH₃⁽¹⁺⁾*BF₄^(1-)=MoI(CO)3P(C₆H₅)2(CH₂)3P(C₆H₅)2(NCCH₃)BF₄

Base Information

• Chemical Name: MoI(CO)3P(C₆H₅)2(CH₂)3P(C₆H₅)2NCCH₃⁽¹⁺⁾*BF₄^(1-)=MoI(CO)3P(C₆H₅)2(CH₂)3P(C₆H₅)2(NCCH₃)BF₄
• CAS No.: 506424-00-6
• Molecular Formula: BF₄*C₃₂H₂₉IMoNO₃P₂
• Molecular Weight: 847.184

Synonyms:

Chemical Property of MoI(CO)3P(C₆H₅)2(CH₂)3P(C₆H₅)2NCCH₃⁽¹⁺⁾*BF₄^(1-)=MoI(CO)3P(C₆H₅)2(CH₂)3P(C₆H₅)2(NCCH₃)BF₄

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Technology Process of MoI(CO)3P(C₆H₅)2(CH₂)3P(C₆H₅)2NCCH₃⁽¹⁺⁾*BF₄^(1-)=MoI(CO)3P(C₆H₅)2(CH₂)3P(C₆H₅)2(NCCH₃)BF₄

There total 1 articles about MoI(CO)3P(C₆H₅)2(CH₂)3P(C₆H₅)2NCCH₃⁽¹⁺⁾*BF₄^(1-)=MoI(CO)3P(C₆H₅)2(CH₂)3P(C₆H₅)2(NCCH₃)BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

silver tetrafluoroborate (14104-20-2) + MoI2(CO)3[(C6H5)2P(CH2)3P(C6H5)2] (73534-52-8) → MoI(CO)3P(C6H5)2(CH2)3P(C6H5)2NCCH3(1+)*BF4(1-)=MoI(CO)3P(C6H5)2(CH2)3P(C6H5)2(NCCH3)BF4 (506424-00-6)

Guidance literature:

In acetonitrile; byproducts: AgI; AgBF4 was added to soln. of Mo-complex in MeCN, stirred for 4 h under N2; solvent was removed under vac., dissolved in CH2Cl2, filtered, solvent was removed in vacuo; elem. anal.;

DOI:10.1016/S0022-328X(02)01894-6

Reference yield: 70.0%

MoI(CO)3P(C6H5)2(CH2)3P(C6H5)2NCCH3(1+)*BF4(1-)=MoI(CO)3P(C6H5)2(CH2)3P(C6H5)2(NCCH3)BF4 (506424-00-6) + bis-diphenylphosphinomethane (2071-20-7) → MoI(CO)2(P(C6H5)2P(C6H5)2)2(CH2)4(1+)*BF4(1-)=MoI(CO)2(P(C6H5)4P)2(CH2)4BF4 (506424-61-9)

Guidance literature:

In dichloromethane; ligand was added to soln. of Mo-complex in CH2Cl2, stirred for 2 h underN2; filtered, solvent was reduced under vac., concd., layered with Et2O, cooled to -17°C for 1 wk; elem. anal.;

DOI:10.1016/S0022-328X(02)01894-6

upstream raw materials:

silver tetrafluoroborate

MoI₂(CO)3[(C₆H₅)2P(CH₂)3P(C₆H₅)2]

Downstream raw materials:

MoI(CO)2(P(C₆H₅)2P(C₆H₅)2)2(CH₂)4⁽¹⁺⁾*BF₄^(1-)=MoI(CO)2(P(C₆H₅)4P)2(CH₂)4BF₄

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