Cu(2,4,6-trimercaptotriazine)(PPh₃)2*CH₂Cl₂

Base Information

Chemical Name:Cu(2,4,6-trimercaptotriazine)(PPh₃)2*CH₂Cl₂
CAS No.:591214-55-0
Molecular Formula:CH₂Cl₂*C₃₉H₃₂CuN₃P₂S₃
Molecular Weight:849.328
Hs Code.:

Cu(2,4,6-trimercaptotriazine)(PPh<sub>3</sub>)2*CH<sub>2</sub>Cl<sub>2</sub>

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Chemical Property of Cu(2,4,6-trimercaptotriazine)(PPh₃)2*CH₂Cl₂

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Technology Process of Cu(2,4,6-trimercaptotriazine)(PPh₃)2*CH₂Cl₂

There total 2 articles about Cu(2,4,6-trimercaptotriazine)(PPh₃)2*CH₂Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 75-09-2
dichloromethane

: sodium 2,4,6-trimercaptotriazine trihydrate

: Cu⁽¹⁺⁾*CH₃CO₂^(1-)*4P(C₆H₅)3=Cu(CH₃CO₂)(P(C₆H₅)3)4

: 591214-55-0
Cu(2,4,6-trimercaptotriazine)(PPh₃)2*CH₂Cl₂

Guidance literature:: In ethanol; EtOH soln. of ligand was added dropwise to EtOH soln. of Cu-complex, stirred at room temp. for 1 h; mother liquor was removed, washed with EtOH, dried in vacuo, recrystd. from CH2Cl2/MeOH; elem. anal.;
DOI:10.1016/S0020-1693(02)01468-8

Reference yield:

: 603-35-0
triphenylphosphine

: 591214-55-0
Cu(2,4,6-trimercaptotriazine)(PPh₃)2*CH₂Cl₂

Guidance literature:: Multi-step reaction with 2 steps

1: methanol

2: dichloromethane

In methanol; dichloromethane;
DOI:10.1016/S0020-1693(02)01468-8