(1'R,2R)-2-Benzyl-1-pyrrolidine

Base Information

Chemical Name:(1'R,2R)-2-Benzyl-1-pyrrolidine
CAS No.:135324-53-7
Molecular Formula:C₁₉H₂₄N₂O
Molecular Weight:296.412
Hs Code.:

(1'R,2R)-2-Benzyl-1-<N-(2-hydroxy-1-phenylethyl)amino>pyrrolidine

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1'R,2R)-2-Benzyl-1-pyrrolidine

Chemical Property:

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Technology Process of (1'R,2R)-2-Benzyl-1-pyrrolidine

There total 5 articles about (1'R,2R)-2-Benzyl-1-pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 135324-47-9,135324-52-6
2-Benzyl-1-(α-ethoxycarbonylbenzylideneamino)pyrrolidine

: 135324-48-0
(1'S,2R)-2-Benzyl-1-pyrrolidine

: 135324-53-7
(1'R,2R)-2-Benzyl-1-pyrrolidine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; Ambient temperature;
DOI:10.1248/cpb.39.836

Reference yield:

: 1603-79-8
phenylglyoxylic acid ethyl ester

: 135324-53-7
(1'R,2R)-2-Benzyl-1-pyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / 60 °C

2: 39 percent / LiAlH₄ / tetrahydrofuran / Ambient temperature

With lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1248/cpb.39.836

Reference yield:

: 63328-13-2
(R)-2-benzylpyrrolidine

: 135324-53-7
(1'R,2R)-2-Benzyl-1-pyrrolidine

Guidance literature:: Multi-step reaction with 4 steps

1: NaNO₂, HOAc / H₂O / 4 h / Ambient temperature

2: LiAlH₄ / tetrahydrofuran / 3 h / Heating

3: 86 percent / 60 °C

4: 39 percent / LiAlH₄ / tetrahydrofuran / Ambient temperature

With lithium aluminium tetrahydride; acetic acid; sodium nitrite; In tetrahydrofuran; water;
DOI:10.1248/cpb.39.836