Rh₂(C₅H₅)2(CO)((C₆H₅)2PCH₂P(C₆H₅)2)(AgO₂CCF₃)

Base Information

Chemical Name:Rh₂(C₅H₅)2(CO)((C₆H₅)2PCH₂P(C₆H₅)2)(AgO₂CCF₃)
CAS No.:101835-32-9
Molecular Formula:C₃₈H₃₂AgF₃O₃P₂Rh₂
Molecular Weight:969.292
Hs Code.:

Rh<sub>2</sub>(C<sub>5</sub>H<sub>5</sub>)2(CO)((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)(AgO<sub>2</sub>CCF<sub>3</sub>)

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Chemical Property of Rh₂(C₅H₅)2(CO)((C₆H₅)2PCH₂P(C₆H₅)2)(AgO₂CCF₃)

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Technology Process of Rh₂(C₅H₅)2(CO)((C₆H₅)2PCH₂P(C₆H₅)2)(AgO₂CCF₃)

There total 2 articles about Rh₂(C₅H₅)2(CO)((C₆H₅)2PCH₂P(C₆H₅)2)(AgO₂CCF₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 88979-33-3
2Rh⁽¹⁺⁾*2C₅H₅^(1-)*CO*(C₆H₅)2PCH₂P(C₆H₅)2=Rh₂(C₅H₅)2(CO)((C₆H₅)2PCH₂P(C₆H₅)2)

: 2966-50-9
silver trifluoroacetate

: 101835-32-9
Rh₂(C₅H₅)2(CO)((C₆H₅)2PCH₂P(C₆H₅)2)(AgO₂CCF₃)

Guidance literature:: In benzene; N2-atmosphere; addn. of a benzene soln. of the Ag salt to a stirred soln. of the Rh complex in benzene; stirring for about 10 min;; pptn. on addn. of Et2O; decantation; recrystn. (CH2Cl2/hexane=1:3); elem. anal.;

Reference yield: 48.5%

: 110682-61-6
bis(η-cyclopentadienyl)(μ-carbonyl)(μ-bis(diphenylphosphino)methane)(μ-copperchloride)dirhodium

: 2966-50-9
silver trifluoroacetate

: 101835-32-9
Rh₂(C₅H₅)2(CO)((C₆H₅)2PCH₂P(C₆H₅)2)(AgO₂CCF₃)

Guidance literature:: In dichloromethane; a CH2Cl2 soln. of Rh2Cu-cluster was treated with a soln. of CF3COOAg in CH2Cl2 under nitrogen, mixt. was stirred for ca. 1 h; evapd., residue was extd. with benzene, Et2O added to the ext., ppt. was recrystd. from CH2Cl2-hexane; elem. anal.;