ZnCl(tetrahydrofuran)2(GaCl(2-[(2,6-diisopropylphenyl)amino]-4-[(2,6-diisopropylphenyl)imino]-2-pentene))

Base Information

• Chemical Name: ZnCl(tetrahydrofuran)2(GaCl(2-[(2,6-diisopropylphenyl)amino]-4-[(2,6-diisopropylphenyl)imino]-2-pentene))
• CAS No.: 958652-02-3
• Molecular Formula: C₃₇H₅₇Cl₂GaN₂O₂Zn
• Molecular Weight: 767.891
• Mol file: 958652-02-3.mol

Synonyms:

Chemical Property of ZnCl(tetrahydrofuran)2(GaCl(2-[(2,6-diisopropylphenyl)amino]-4-[(2,6-diisopropylphenyl)imino]-2-pentene))

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ZnCl(tetrahydrofuran)2(GaCl(2-[(2,6-diisopropylphenyl)amino]-4-[(2,6-diisopropylphenyl)imino]-2-pentene))

There total 1 articles about ZnCl(tetrahydrofuran)2(GaCl(2-[(2,6-diisopropylphenyl)amino]-4-[(2,6-diisopropylphenyl)imino]-2-pentene)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + [Ga(2-((2,6-diisoproylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-2-pentene)] (317322-17-1) + zinc(II) chloride (7646-85-7,24359-56-6) → ZnCl(tetrahydrofuran)2(GaCl(2-[(2,6-diisopropylphenyl)amino]-4-[(2,6-diisopropylphenyl)imino]-2-pentene)) (958652-02-3) + Zn(GaCl(2-[(2,6-diisopropylphenyl)amino]-4-[(2,6-diisopropylphenyl)imino]-2-pentene))2

Guidance literature:

In tetrahydrofuran; (Ar); stirring soln. of zinc compd. and gallium compd. in THF at room temp. for 1 h; concg., keeping at -30°C overnight, isolation of crystals, elem. anal.;

DOI:10.1021/ic7013804

Reference yield: 72.0%

ZnCl(tetrahydrofuran)2(GaCl(2-[(2,6-diisopropylphenyl)amino]-4-[(2,6-diisopropylphenyl)imino]-2-pentene)) (958652-02-3) + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) → [ZnCl(tetrahydrofuran)(Ga(tetrahydrofuran)(2-[(2,6-diisopropylphenyl)amino]-4-[(2,6-diisopropylphenyl)imino]-2-pentene))]2(BArF)2

Guidance literature:

In tetrahydrofuran; (Ar); stirring mixt. of zinc compd. and borate deriv. salt in THF at room temp. for 1 h; keeping at -30°C overnight, isolation of crystals, elem. anal.;

DOI:10.1021/ic7013804

upstream raw materials:

tetrahydrofuran

[Ga(2-((2,6-diisoproylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-2-pentene)]

zinc(II) chloride