lithium 7,7,8,8-tetracyanoquinodimethane

Base Information

• Chemical Name: lithium 7,7,8,8-tetracyanoquinodimethane
• CAS No.: 34507-61-4
• Molecular Formula: C₁₂H₄N₄*Li
• Molecular Weight: 211.132

Synonyms:

Chemical Property of lithium 7,7,8,8-tetracyanoquinodimethane

Chemical Property:

Purity/Quality:

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Technology Process of lithium 7,7,8,8-tetracyanoquinodimethane

There total 3 articles about lithium 7,7,8,8-tetracyanoquinodimethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

7,7,8,8-tetracyanoquinodimethane + lithium iodide (10377-51-2) → lithium 7,7,8,8-tetracyanoquinodimethane (34507-61-4,1283-90-5)

Guidance literature:

In acetonitrile; for 0.0833333h; Inert atmosphere; Reflux;

DOI:10.1021/acs.inorgchem.5b00808

Reference yield: 96.0%

7,7',8,8'-tetracyanoquinodimethane (1518-16-7,6144-37-2) → lithium 7,7,8,8-tetracyanoquinodimethane (34507-61-4,1283-90-5)

Guidance literature:

With lithium iodide; In acetonitrile; for 2h; Inert atmosphere; Reflux;

DOI:10.1039/C6RA21636F

Reference yield:

2-amino-4,6-diethyl-1,3,5-trimethylborazine (135225-73-9) + 1,3,5-Trimethyl-2,4,6-tris-methylsulfanyl-[1,3,5,2,4,6]triazatriborinane (61423-62-9) → lithium 7,7,8,8-tetracyanoquinodimethane (34507-61-4,1283-90-5)

Guidance literature:

stirred mixt. was heated for 20 h in bath of 75-80°C; mixt. was cooled to room temp., dissolved in boiling hexane;

upstream raw materials:

2-amino-4,6-diethyl-1,3,5-trimethylborazine

1,3,5-Trimethyl-2,4,6-tris-methylsulfanyl-[1,3,5,2,4,6]triazatriborinane

lithium iodide

7,7',8,8'-tetracyanoquinodimethane

Downstream raw materials:

1,2-bis<4-(α,α-dicyano-p-N,N-dimethylaminobenzyl)phenyl>-1,1,2,2-tetracyanoethane

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