Technology Process of C22H27N6O6P
There total 5 articles about C22H27N6O6P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
methanol;
for 3h;
Heating;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / diethyl ether / 1.) 0-10 deg C, 5 h, 2.) r.t., 12 h
2: 30 percent / N-methylpiperidine, N-methyl-pyrrolidone / 24 h / 150 °C
3: H2 / 10 percent Pd/C / methanol
4: 22 percent / p-toluenesulfonic acid / methanol / 3 h / Heating
With
1-methyl-pyrrolidin-2-one; N-methylcyclohexylamine; hydrogen; toluene-4-sulfonic acid; triethylamine;
palladium on activated charcoal;
In
methanol; diethyl ether;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / diethyl ether / 1.) 0-10 deg C, 5 h, 2.) r.t., 12 h
2: 30 percent / N-methylpiperidine, N-methyl-pyrrolidone / 24 h / 150 °C
3: H2 / 10 percent Pd/C / methanol
4: 22 percent / p-toluenesulfonic acid / methanol / 3 h / Heating
With
1-methyl-pyrrolidin-2-one; N-methylcyclohexylamine; hydrogen; toluene-4-sulfonic acid; triethylamine;
palladium on activated charcoal;
In
methanol; diethyl ether;