menthyl glycinate hydrochloride

Base Information

Chemical Name:menthyl glycinate hydrochloride
CAS No.:91694-30-3
Molecular Formula:C₁₂H₂₃NO₂*ClH
Molecular Weight:249.781
Hs Code.:

Synonyms:

Suppliers and Price of menthyl glycinate hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of menthyl glycinate hydrochloride

Chemical Property:

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Technology Process of menthyl glycinate hydrochloride

There total 1 articles about menthyl glycinate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15356-70-4
menthol

: 56-40-6,18875-39-3,25718-94-9
glycine

: 91694-30-3,125424-05-7,125424-06-8
menthyl glycinate hydrochloride

Guidance literature:: With hydrogenchloride; toluene-4-sulfonic acid; Yield given. Multistep reaction; 1.) benzene, reflux, 2.) ether;
DOI:10.1021/ja00369a036

Reference yield:

: 91694-30-3,125424-05-7,125424-06-8
menthyl glycinate hydrochloride

: 80594-25-8
dl-menthyl α-deuteriodiazoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) acetic acid, 2.) isoamyl nitrite / 2.) benzene, reflux, 6 h

2: 84 percent / sodium deuteroxide, benzylhexadecyldimethylammonium chloride / CH₂Cl₂; D₂O / 48 h

With deuteriated sodium hydroxide; cetyldimethylbenzylammonium chloride; acetic acid; isopentyl nitrite; In dichloromethane; water-d2;
DOI:10.1021/ja00369a036

Reference yield:

: 91694-30-3,125424-05-7,125424-06-8
menthyl glycinate hydrochloride

: 80594-23-6
menthyl c-2-phenyl-1,2,t-3-trideuteriocyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) acetic acid, 2.) isoamyl nitrite / 2.) benzene, reflux, 6 h

2: 84 percent / sodium deuteroxide, benzylhexadecyldimethylammonium chloride / CH₂Cl₂; D₂O / 48 h

3: (+)-(R)-2-<2,2-bis(5-tert-butyl-2-heptylphenyl)-2-hydroxy-1-methylethylimino>methylphenolcopper complex / cyclohexane / 9 h / 75 °C

With deuteriated sodium hydroxide; (+)-(R)-2-<2,2-bis(5-tert-butyl-2-heptylphenyl)-2-hydroxy-1-methylethylimino>methylphenolcopper; cetyldimethylbenzylammonium chloride; acetic acid; isopentyl nitrite; In dichloromethane; cyclohexane; water-d2;
DOI:10.1021/ja00369a036