1-Benzyloxy-9-decene

Base Information

• Chemical Name: 1-Benzyloxy-9-decene
• CAS No.: 100189-71-7
• Molecular Formula: C17H26O
• Molecular Weight: 246.393
• DSSTox Substance ID: DTXSID30464095
• Nikkaji Number: J2.212.838H
• Wikidata: Q82289287
• Mol file: 100189-71-7.mol

Synonyms:1-Benzyloxy-9-decene;100189-71-7;dec-9-enoxymethylbenzene;dec-9-enyloxymethylbenzene;SCHEMBL4104428;DTXSID30464095;ZOPVCRZGFUSKEF-UHFFFAOYSA-N

Chemical Property of 1-Benzyloxy-9-decene

Chemical Property:

• XLogP3: 5.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 11
• Exact Mass: 246.198365449
• Heavy Atom Count: 18
• Complexity: 182

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CCCCCCCCCOCC1=CC=CC=C1

Technology Process of 1-Benzyloxy-9-decene

There total 3 articles about 1-Benzyloxy-9-decene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

9-Decen-1-ol (13019-22-2) + benzyl bromide (100-39-0) → ((dec-9-en-1-yloxy)methyl)benzene (100189-71-7)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2.25h;

DOI:10.1021/jo0303721

Reference yield: 83.0%

9-Decen-1-ol (13019-22-2) + benzyl chloride (100-44-7) → ((dec-9-en-1-yloxy)methyl)benzene (100189-71-7)

Guidance literature:

9-Decen-1-ol; With sodium hydride; In tetrahydrofuran; at 20 ℃;

benzyl chloride; In tetrahydrofuran; for 16h; Heating;

DOI:10.1016/S0009-3084(03)00043-4

Reference yield:

→ ((dec-9-en-1-yloxy)methyl)benzene (100189-71-7)

Guidance literature:

With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.333333h;

With potassium iodide; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 16h;

upstream raw materials:

9-Decen-1-ol

benzyl bromide

benzyl chloride

Downstream raw materials:

2-[8-(benzyloxy)octyl]oxirane

(R)-10-(benzyloxy)decane-1,2-diol

2-azido-10-(benzyloxy)-1-iododecane

1-Decanol