2-methyl-10-(phenylmethoxy)decanal

Base Information

• Chemical Name: 2-methyl-10-(phenylmethoxy)decanal
• CAS No.: 1227407-06-8
• Molecular Formula: C₁₈H₂₈O₂
• Molecular Weight: 276.419
• Mol file: 1227407-06-8.mol

Synonyms:

Chemical Property of 2-methyl-10-(phenylmethoxy)decanal

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-methyl-10-(phenylmethoxy)decanal

There total 2 articles about 2-methyl-10-(phenylmethoxy)decanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + ((dec-9-en-1-yloxy)methyl)benzene (100189-71-7) → 2-methyl-10-(phenylmethoxy)decanal (1227407-06-8) + 11-(phenylmethoxy)undecanal (1227407-05-7)

Guidance literature:

With chloro(1,5-cyclooctadiene)rhodium(I) dimer; 2,2'-bis(diphenylphosphino)biphenyl; nixantphos; In toluene; at 90 ℃; for 20h; regioselective reaction; Inert atmosphere;

DOI:10.1002/adsc.200900713

Reference yield:

formic acid (64-18-6) + ((dec-9-en-1-yloxy)methyl)benzene (100189-71-7) → 2-methyl-10-(phenylmethoxy)decanal (1227407-06-8) + 11-(phenylmethoxy)undecanal (1227407-05-7)

Guidance literature:

With 1,3-bis-(diphenylphosphino)propane; palladium diacetate; acetic anhydride; tetra-(n-butyl)ammonium iodide; In 1,2-dichloro-ethane; at 80 ℃; for 24h; Overall yield = 52 %; regioselective reaction; Inert atmosphere; Molecular sieve;

DOI:10.1021/jacs.6b10297

upstream raw materials:

formaldehyd

((dec-9-en-1-yloxy)methyl)benzene

formic acid