methyl 2,6-anhydro-2-C--3-deoxy-4,5:7,8-bis-O-(isopropylidene)-D-glycero-D-talo-octonate

Base Information

Chemical Name:methyl 2,6-anhydro-2-C--3-deoxy-4,5:7,8-bis-O-(isopropylidene)-D-glycero-D-talo-octonate
CAS No.:126709-04-4
Molecular Formula:C₄₁H₄₉ClN₃O₁₆P
Molecular Weight:906.277
Hs Code.:

methyl 2,6-anhydro-2-C-<N-benzoyl-P-(2-chlorophenyl)-2',3'-O-(isopropylidene)-(5'-cytidylyloxy)methyl>-3-deoxy-4,5:7,8-bis-O-(isopropylidene)-D-glycero-D-talo-octonate

Synonyms:

Suppliers and Price of methyl 2,6-anhydro-2-C--3-deoxy-4,5:7,8-bis-O-(isopropylidene)-D-glycero-D-talo-octonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,6-anhydro-2-C--3-deoxy-4,5:7,8-bis-O-(isopropylidene)-D-glycero-D-talo-octonate

Chemical Property:

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Technology Process of methyl 2,6-anhydro-2-C--3-deoxy-4,5:7,8-bis-O-(isopropylidene)-D-glycero-D-talo-octonate

There total 2 articles about methyl 2,6-anhydro-2-C--3-deoxy-4,5:7,8-bis-O-(isopropylidene)-D-glycero-D-talo-octonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15074-54-1
2-chlorophenyl dichlorophosphate

: 126709-04-4,126786-11-6
methyl 2,6-anhydro-2-C--3-deoxy-4,5:7,8-bis-O-(isopropylidene)-D-glycero-D-talo-octonate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / acetonitrile

2: 4-dimethylaminopyridine / pyridine / 1.5 h

With dmap; triethylamine; In pyridine; acetonitrile;
DOI:10.1016/0223-5234(89)90090-1

Reference yield:

: 72351-28-1
2-chlorophenyl phosphordi(1H-1-[1,2,4]triazolide)

: 107961-78-4,107961-79-5
2,6-anhydro-3-deoxy-2-(hydroxymethyl)-4,5:7,8-di-O-isopropylidene-D-glycero-D-talo-octonate

: 39946-94-6,98807-30-8
4-N-benzoyl-2',3'-O-isopropylidenecytidine

: 126709-04-4,126786-11-6
methyl 2,6-anhydro-2-C--3-deoxy-4,5:7,8-bis-O-(isopropylidene)-D-glycero-D-talo-octonate

: 126709-05-5
bis-2-chlorophenylphosphate

Guidance literature:: With dmap; In pyridine; for 1.5h; Yield given. Yields of byproduct given;
DOI:10.1016/0223-5234(89)90090-1

Reference yield:

: 126709-04-4,126786-11-6
methyl 2,6-anhydro-2-C--3-deoxy-4,5:7,8-bis-O-(isopropylidene)-D-glycero-D-talo-octonate

: 126709-03-3
2,6-anhydro-2-C-<(5'-cytidylyloxy)methyl>-3-deoxy-D-glycero-D-talo-octonic acid

Guidance literature:: With sodium hydroxide; 1,1,3,3-tetramethylguanidine; trifluoroacetic acid; 4-nitrobenzaldehyde oxime; Yield given. Multistep reaction; 1.) water: dioxane, 24 h; 2.) rt; 3.) 50 min;
DOI:10.1016/0223-5234(89)90090-1