Technology Process of 2(2-ethyloxy-5-ethylenedioxycyclohexyl)-1,3-dimethoxy-5-pentylbenzene
There total 10 articles about 2(2-ethyloxy-5-ethylenedioxycyclohexyl)-1,3-dimethoxy-5-pentylbenzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
diethyl ether;
for 6h;
Heating;
DOI:10.1139/v82-047
- Guidance literature:
-
Multi-step reaction with 10 steps
1: n-BuLi
2: 87 percent / piperidine
3: 99 percent / benzene / 2 h / Heating
4: 94 percent / 6N hydrochloric acid / acetone / 0.75 h / Ambient temperature
5: 91 percent / p-toluenesulfonic acid / benzene / 2.5 h / Heating
6: 99 percent / 10percent palladium on charcoal, hydrogen / ethanol / 6 h
7: 93 percent / p-toluenesulfonic acid / benzene / 4 h / Heating
8: 94 percent / 10N aqueous sodium hydroxide / ethanol / 20 h / Heating
9: 88 percent / sodium hydroxide / dimethylformamide / 8 h / Heating
10: 40 percent / diethyl ether / 6 h / Heating
With
piperidine; hydrogenchloride; sodium hydroxide; palladium on activated charcoal; n-butyllithium; hydrogen; toluene-4-sulfonic acid;
In
diethyl ether; ethanol; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1139/v82-047
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 87 percent / piperidine
2: 99 percent / benzene / 2 h / Heating
3: 94 percent / 6N hydrochloric acid / acetone / 0.75 h / Ambient temperature
4: 91 percent / p-toluenesulfonic acid / benzene / 2.5 h / Heating
5: 99 percent / 10percent palladium on charcoal, hydrogen / ethanol / 6 h
6: 93 percent / p-toluenesulfonic acid / benzene / 4 h / Heating
7: 94 percent / 10N aqueous sodium hydroxide / ethanol / 20 h / Heating
8: 88 percent / sodium hydroxide / dimethylformamide / 8 h / Heating
9: 40 percent / diethyl ether / 6 h / Heating
With
piperidine; hydrogenchloride; sodium hydroxide; palladium on activated charcoal; hydrogen; toluene-4-sulfonic acid;
In
diethyl ether; ethanol; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1139/v82-047
