Methyl 2-acetyl-4-ethoxy-5-methoxybenzeneacetate

Base Information

Chemical Name:Methyl 2-acetyl-4-ethoxy-5-methoxybenzeneacetate
CAS No.:171814-31-6
Molecular Formula:C₁₄H₁₈O₅
Molecular Weight:266.294
Hs Code.:
DSSTox Substance ID:DTXSID401238280

Synonyms:DTXSID401238280;Methyl 2-acetyl-4-ethoxy-5-methoxybenzeneacetate;171814-31-6

Suppliers and Price of Methyl 2-acetyl-4-ethoxy-5-methoxybenzeneacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 2-acetyl-4-ethoxy-5-methoxybenzeneacetate

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:7
Exact Mass:266.11542367
Heavy Atom Count:19
Complexity:315

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC1=C(C=C(C(=C1)C(=O)C)CC(=O)OC)OC

Technology Process of Methyl 2-acetyl-4-ethoxy-5-methoxybenzeneacetate

There total 2 articles about Methyl 2-acetyl-4-ethoxy-5-methoxybenzeneacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 55761-07-4
methyl 4-ethoxy-3-methoxyphenylacetate

: 75-36-5
acetyl chloride

: 171814-31-6
methyl 6-acetyl-4-ethoxy-3-methoxyphenylacetate

Guidance literature:: With aluminium trichloride; In 1,2-dichloro-ethane; a) 68 deg C, 3 h, b) RT, 16 h;
DOI:10.1002/jhet.5570320450

Reference yield:

: 120-13-8
4-ethoxy-3-methoxyphenylacetic acid

: 171814-31-6
methyl 6-acetyl-4-ethoxy-3-methoxyphenylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / conc. H₂SO₄ / 21 h / 68 °C

2: 65 percent / AlCl₃ / 1,2-dichloro-ethane / a) 68 deg C, 3 h, b) RT, 16 h

With aluminium trichloride; sulfuric acid; In 1,2-dichloro-ethane;
DOI:10.1002/jhet.5570320450