2-Phenylamino-5--1,3,4-thiadiazole

Base Information

Chemical Name:2-Phenylamino-5--1,3,4-thiadiazole
CAS No.:116270-69-0
Molecular Formula:C₃₀H₂₄N₆OS
Molecular Weight:516.626
Hs Code.:

2-Phenylamino-5-<p-(3-o-tolyl-4-oxoquinazolin-2-ylmethylamino)phenyl>-1,3,4-thiadiazole

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Phenylamino-5--1,3,4-thiadiazole

Chemical Property:

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Technology Process of 2-Phenylamino-5--1,3,4-thiadiazole

There total 5 articles about 2-Phenylamino-5--1,3,4-thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 116285-50-8
N¹--N⁴-phenylthiosemicarbazide

: 116270-69-0
2-Phenylamino-5--1,3,4-thiadiazole

Guidance literature:: With sulfuric acid; for 4h; Ambient temperature;

Reference yield:

: 4-[(4-Oxo-3-o-tolyl-3,4-dihydro-quinazolin-2-ylmethyl)-amino]-benzoic acid ethyl ester

: 116270-69-0
2-Phenylamino-5--1,3,4-thiadiazole

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / ethanol / 12 h / Heating

2: 63 percent / ethanol / 6 h / Heating

3: 60 percent / conc. sulphuric acid / 4 h / Ambient temperature

With sulfuric acid; hydrazine hydrate; In ethanol;

Reference yield:

: 116270-54-3
2-<(p-Hydrazinocarbonyl)phenylaminomethyl>-3-(o-tolyl)quinazolin-4(3H)-one

: 116270-69-0
2-Phenylamino-5--1,3,4-thiadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / ethanol / 6 h / Heating

2: 60 percent / conc. sulphuric acid / 4 h / Ambient temperature

With sulfuric acid; In ethanol;