C₂₅H₂₈Cl₂NO₅PS

Base Information

Chemical Name:C₂₅H₂₈Cl₂NO₅PS
CAS No.:1447961-22-9
Molecular Formula:C₂₅H₂₈Cl₂NO₅PS
Molecular Weight:556.447
Hs Code.:

C<sub>25</sub>H<sub>28</sub>Cl<sub>2</sub>NO<sub>5</sub>PS

Synonyms:

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Chemical Property of C₂₅H₂₈Cl₂NO₅PS

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Technology Process of C₂₅H₂₈Cl₂NO₅PS

There total 6 articles about C₂₅H₂₈Cl₂NO₅PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1447961-11-6
diethyl (3-(N-(benzyloxy)-2-(thiophen-2-ylmethyl)benzamido)-1-(3,4-dichlorophenyl)propyl)phosphonate

: 1447961-22-9
C₂₅H₂₈Cl₂NO₅PS

Guidance literature:: With trimethylsilyl bromide; methyl-phenyl-thioether; trifluoroacetic acid; In methanol; for 22h; under 760.051 Torr; Cooling with ice;
DOI:10.1021/jm4006498

Reference yield:

: 62636-87-7
2-(thiophene-2-yl-methyl)-benzoic acid

: 1447961-22-9
C₂₅H₂₈Cl₂NO₅PS

Guidance literature:: Multi-step reaction with 2 steps

1: ammonia; zinc / ethyl acetate / 48 h / Reflux

2: trimethylsilyl bromide; trifluoroacetic acid; methyl-phenyl-thioether / methanol / 22 h / 760.05 Torr / Cooling with ice

With trimethylsilyl bromide; methyl-phenyl-thioether; ammonia; trifluoroacetic acid; zinc; In methanol; ethyl acetate;
DOI:10.1021/jm4006498

Reference yield:

: 151169-75-4
3,4-dichlophenylboronic acid

: 1447961-22-9
C₂₅H₂₈Cl₂NO₅PS

Guidance literature:: Multi-step reaction with 5 steps

1.1: palladium diacetate; p-benzoquinone; 2.9-dimethyl-1,10-phenanthroline / 100 °C / Microwave irradiation

2.1: phenol / 100 °C

2.2: 100 °C

3.1: pyridine / ethanol / 20 °C

3.2: 20 °C

4.1: ammonia; zinc / ethyl acetate / 48 h / Reflux

5.1: trimethylsilyl bromide; trifluoroacetic acid; methyl-phenyl-thioether / methanol / 22 h / 760.05 Torr / Cooling with ice

With pyridine; 2.9-dimethyl-1,10-phenanthroline; trimethylsilyl bromide; methyl-phenyl-thioether; ammonia; palladium diacetate; trifluoroacetic acid; p-benzoquinone; zinc; phenol; In methanol; ethanol; ethyl acetate; 1.1: |Heck Reaction;
DOI:10.1021/jm4006498