3-chloro-4-nitrobenzyl ethyl ether

Base Information

• Chemical Name: 3-chloro-4-nitrobenzyl ethyl ether
• CAS No.: 77455-64-2
• Molecular Formula: C₉H₁₀ClNO₃
• Molecular Weight: 215.636

Synonyms:

Chemical Property of 3-chloro-4-nitrobenzyl ethyl ether

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 3-chloro-4-nitrobenzyl ethyl ether

There total 3 articles about 3-chloro-4-nitrobenzyl ethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

ethanol (64-17-5) + 3-chloro-4-nitrobenzylidene dichloride (77455-58-4) → 3-chloro-4-nitrobenzyl chloride (77455-59-5) + 3-chloro-4-nitrobenzyl ethyl ether (77455-64-2) + 3,3'-dichloro-4,4'-dinitrodiphenylacetylene (77455-63-1) + 1,2-bis-(3-chloro-4-nitrophenyl)tetrachloroethane (77455-60-8) + (Z)-α,α',3,3'-tetrachloro-4,4'-dinitrostilbene (77455-62-0) + (E)-α,α',3,3'-tetrachloro-4,4'-dinitrostilbene (77455-61-9)

Guidance literature:

With potassium hydroxide; In water; at 28 ℃; for 0.4h; Mechanism;

DOI:10.1039/P19810000423

Reference yield:

ethanol (64-17-5) + 3-chloro-4-nitrobenzylidene dichloride (77455-58-4) → 3-chloro-4-nitrobenzyl ethyl ether (77455-64-2) + 1,2-bis-(3-chloro-4-nitrophenyl)tetrachloroethane (77455-60-8) + (Z)-α,α',3,3'-tetrachloro-4,4'-dinitrostilbene (77455-62-0) + (E)-α,α',3,3'-tetrachloro-4,4'-dinitrostilbene (77455-61-9)

Guidance literature:

With potassium hydroxide; In water; at 28 ℃; for 0.4h; Further byproducts given. Yields of byproduct given;

DOI:10.1039/P19810000423

Reference yield:

→ 3-chloro-4-nitrobenzyl ethyl ether (77455-64-2)

Guidance literature:

upstream raw materials:

ethanol

3-chloro-4-nitrobenzylidene dichloride

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