6-nitroindole-3-glyoxylic acid

Base Information

Chemical Name:6-nitroindole-3-glyoxylic acid
CAS No.:90947-21-0
Molecular Formula:C₁₀H₆N₂O₅
Molecular Weight:234.168
Hs Code.:

Synonyms:

Suppliers and Price of 6-nitroindole-3-glyoxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
2-(6-Nitro-3-indolyl)-2-oxoaceticAcid
1g
$ 802.00

Total 1 raw suppliers

Chemical Property of 6-nitroindole-3-glyoxylic acid

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

2-(6-Nitro-3-indolyl)-2-oxoaceticAcid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-nitroindole-3-glyoxylic acid

There total 5 articles about 6-nitroindole-3-glyoxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 133053-91-5
methyl 6-nitroindole-3-glyoxylate

: 90947-21-0
6-nitroindole-3-glyoxylic acid

Guidance literature:: With potassium hydroxide; In ethanol; water; for 1.5h; Heating;
DOI:10.1016/S0040-4020(01)87932-1

Reference yield:

: 36192-16-2
N'-(2-methyl-5-nitrophenyl)-N,N-dimethylformamidine

: 90947-21-0
6-nitroindole-3-glyoxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1) potassium tert-butoxide, 2) acetic acid / 1) DMF, 45 min, on a steam bath, 2) H₂O, 10 min, reflux

2: 96 percent / potassium hydroxide / ethanol; H₂O / 1.5 h / Heating

With potassium hydroxide; potassium tert-butylate; acetic acid; In ethanol; water;
DOI:10.1016/S0040-4020(01)87932-1

Reference yield:

: 99-55-8
2-methyl-5-nitroaniline

: 90947-21-0
6-nitroindole-3-glyoxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / phosphorus oxychloride / 2 h / heated on a steam bath

2: 1) potassium tert-butoxide, 2) acetic acid / 1) DMF, 45 min, on a steam bath, 2) H₂O, 10 min, reflux

3: 96 percent / potassium hydroxide / ethanol; H₂O / 1.5 h / Heating

With potassium hydroxide; potassium tert-butylate; acetic acid; trichlorophosphate; In ethanol; water;
DOI:10.1016/S0040-4020(01)87932-1