6-o-tolylquinoline-3-carbaldehyde

Base Information

Chemical Name:6-o-tolylquinoline-3-carbaldehyde
CAS No.:1350888-22-0
Molecular Formula:C₁₇H₁₃NO
Molecular Weight:247.296
Hs Code.:

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Suppliers and Price of 6-o-tolylquinoline-3-carbaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-o-tolylquinoline-3-carbaldehyde

Chemical Property:

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Technology Process of 6-o-tolylquinoline-3-carbaldehyde

There total 6 articles about 6-o-tolylquinoline-3-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1350888-21-9
(6-o-tolylquinolin-3-yl)methanol

: 1350888-22-0
6-o-tolylquinoline-3-carbaldehyde

Guidance literature:: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; In dichloromethane; for 1h; Inert atmosphere;
DOI:10.1021/jm200544q

Reference yield:

: 1220418-77-8
6-bromoquinoline-3-carboxylic acid methyl ester

: 1350888-22-0
6-o-tolylquinoline-3-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / ethanol / 0.17 h / 120 °C / Inert atmosphere; Microwave irradiation

2: diisobutylaluminium hydride / hexane; dichloromethane / 1.5 h / Inert atmosphere; Cooling with ice

3: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 1 h / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrapropylammonium perruthennate; diisobutylaluminium hydride; potassium carbonate; 4-methylmorpholine N-oxide; In ethanol; hexane; dichloromethane; 1: Suzuki coupling;
DOI:10.1021/jm200544q

Reference yield:

: methyl 6-o-tolylquinoline-3-carboxylate

: 1350888-22-0
6-o-tolylquinoline-3-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / hexane; dichloromethane / 1.5 h / Inert atmosphere; Cooling with ice

2: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 1 h / Inert atmosphere

With tetrapropylammonium perruthennate; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; In hexane; dichloromethane;
DOI:10.1021/jm200544q