bis(2,2'-bipyridine)-5-(2,5-dimethoxyphenyl)acetylamino-1,10-phenanthroline ruthenium(II) hexafluorophosphate

Base Information

Chemical Name:bis(2,2'-bipyridine)-5-(2,5-dimethoxyphenyl)acetylamino-1,10-phenanthroline ruthenium(II) hexafluorophosphate
CAS No.:112219-94-0
Molecular Formula:C₄₂H₃₅N₇O₃Ru*2F₆P
Molecular Weight:1076.78
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(2,2'-bipyridine)-5-(2,5-dimethoxyphenyl)acetylamino-1,10-phenanthroline ruthenium(II) hexafluorophosphate

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Technology Process of bis(2,2'-bipyridine)-5-(2,5-dimethoxyphenyl)acetylamino-1,10-phenanthroline ruthenium(II) hexafluorophosphate

There total 1 articles about bis(2,2'-bipyridine)-5-(2,5-dimethoxyphenyl)acetylamino-1,10-phenanthroline ruthenium(II) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: ammonium hexafluorophosphate

: 84537-86-0
bis(2,2′-bipyridine)(5-aminophenanthroline)ruthenium bis(hexafluorophosphate)

: 52711-92-9
2,5-dimethoxyphenylacetyl chloride

: 112219-94-0
bis(2,2'-bipyridine)-5-(2,5-dimethoxyphenyl)acetylamino-1,10-phenanthroline ruthenium(II) hexafluorophosphate

Guidance literature:: With (C₂H₅)3N; In dichloromethane; soln. of (bpy)2Ru(5-AP)(PF6)2, triethylamine and 2,5-dimethoxyphenylacetyl chloride in CH2Cl2 stirred for 2 d at 25 ° C and refluxed for 2 h; solvent removed and residue dissolved in H2O and pptd. with NH4PF6; crude powder dried under vacuum and chromatographed on Al2O3 using 30% CH3CN/CH2Cl2; purified RuDMB dissolved in CH3CN and pptd. from diethyl ether;
DOI:10.1021/ja00212a029