[Ir2(CH3)(CO)3(μ-dimethyl acetylendicarboxylate)(dppm)2](CF3SO3)

Base Information

Chemical Name:[Ir2(CH3)(CO)3(μ-dimethyl acetylendicarboxylate)(dppm)2](CF3SO3)
CAS No.:173197-63-2
Molecular Formula:CF₃O₃S*C₆₀H₅₃Ir₂O₇P₄
Molecular Weight:1543.48
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Chemical Property of [Ir2(CH3)(CO)3(μ-dimethyl acetylendicarboxylate)(dppm)2](CF3SO3)

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Technology Process of [Ir2(CH3)(CO)3(μ-dimethyl acetylendicarboxylate)(dppm)2](CF3SO3)

There total 3 articles about [Ir2(CH3)(CO)3(μ-dimethyl acetylendicarboxylate)(dppm)2](CF3SO3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: [Ir2(CH3)(CO)2(μ-η(1):η(1)-dimethyl acetylenedicarboxylate)(bis(diphenylphosphino)methane)2][SO3CF3]

: 201230-82-2
carbon monoxide

: 173197-63-2,248938-63-8
[Ir2(CH3)(CO)3(μ-dimethyl acetylendicarboxylate)(dppm)2](CF3SO3)

Guidance literature:: In dichloromethane; bubbling CO through soln. of Ir-complex for 30 s, stirring for 5 min under CO; concn., pptn. on addn. of Et2O, washing (Et2O), drying (vac.), recrystn.(CH2Cl2:Et2O); elem. anal.;
DOI:10.1021/om990291o