(N,N-dimethylaniline)tricarbonylchromium

Base Information

Chemical Name:(N,N-dimethylaniline)tricarbonylchromium
CAS No.:124916-48-9
Molecular Formula:C₁₁H₁₁CrNO₃
Molecular Weight:257.209
Hs Code.:

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Chemical Property of (N,N-dimethylaniline)tricarbonylchromium

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Technology Process of (N,N-dimethylaniline)tricarbonylchromium

There total 1 articles about (N,N-dimethylaniline)tricarbonylchromium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 77490-97-2
tricarbonyl[η(6)-(N,N-dimethylamino)anisole]chromium

: 22560-16-3
lithium triethylborohydride

: 12116-44-8
(η6-anisol)tricarbonyl chromium

: 124916-48-9,14122-95-3,12109-10-3
(N,N-dimethylaniline)tricarbonylchromium

Guidance literature:: With trifluoroacetic acid; In tetrahydrofuran; addn. of known excess of Et3BHLi to N,N-dimethylaminoarenetricarbonylchromium (THF, room temp.), stirring (several h, N2), addn. to a soln. of CF3CO2H (THF, excess); extn., neutralization, sepn. (silica gel flash chromy.), recrystn. (acetone/light petroleum);
DOI:10.1039/c39910001634

Reference yield: 75.0%

: 124916-48-9,14122-95-3,12109-10-3
(N,N-dimethylaniline)tricarbonylchromium

: 81290-20-2
(trifluoromethyl)trimethylsilane

: 329-00-0
N,N-dimethyl-3-trifluoromethylaniline

Guidance literature:: (N,N-dimethylaniline)tricarbonylchromium; (trifluoromethyl)trimethylsilane; With tetramethylammonium fluoride; In 1,2-dimethoxyethane; at -10 ℃; for 1.75h; Inert atmosphere; Schlenk technique;

With p-benzoquinone; In 1,2-dimethoxyethane; at -60 ℃; for 4h; Reagent/catalyst; Inert atmosphere; Schlenk technique;
DOI:10.1039/c6cc09905j

Reference yield: 54.0%

: potassium cyanide

: 124916-48-9,14122-95-3,12109-10-3
(N,N-dimethylaniline)tricarbonylchromium

: 98-88-4
benzoyl chloride

: 80080-34-8
(η6-C6H5N(CH3)2)Cr(CO)2CNCOC6H5

Guidance literature:: In methanol; acetone; Irradiation (UV/VIS); N2 bubbled through the methanol soln. of Cr-compd. and KCN for 15 min, soln. was irradiated, soln. chromd., solvent evapd., acetone soln. of C6H5COCl added; soln. chromd. two times, residue sepd., product recrystd.; elem. anal.;