ethylene glycol 1-amino-2-phenylethane-1-boronate

Base Information

Chemical Name:ethylene glycol 1-amino-2-phenylethane-1-boronate
CAS No.:88765-82-6
Molecular Formula:C₁₀H₁₄BNO₂
Molecular Weight:191.038
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethylene glycol 1-amino-2-phenylethane-1-boronate

Chemical Property:

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Technology Process of ethylene glycol 1-amino-2-phenylethane-1-boronate

There total 2 articles about ethylene glycol 1-amino-2-phenylethane-1-boronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88765-79-1
ethylene glycol 1-(bis(trimethylsilyl)amino)-2-phenylethane-1-boronate

: 88765-82-6
ethylene glycol 1-amino-2-phenylethane-1-boronate

Guidance literature:: With methanol; In diethyl ether; a soln. of boronate in ether at 0°C was treated with cold (0°C) methanol and stirred under Ar for 45 min at 0°C; anal. purity of the product was not achieved; solvent was distilled under vac. at up to 30°C, residue was treated with ether and collected; elem. anal.;
DOI:10.1021/om00082a019

Reference yield:

: 88765-78-0
ethylene glycol 1-chloro-2-phenylethane-1-boronate

: 88765-82-6
ethylene glycol 1-amino-2-phenylethane-1-boronate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: methanol

In tetrahydrofuran; methanol;
DOI:10.1021/ja00407a051

Reference yield:

: 88765-82-6
ethylene glycol 1-amino-2-phenylethane-1-boronate

: 88765-86-0
1-amino-2-phenylethane-1-boronic acid

Guidance literature:: With water; In diethyl ether; dioxaborol was treated with water and ether; aq. phase was extd. with ether, ether and suspended solid were washed with an addnl. small amt. of water, partially concd., solid was filtered,examined by (1)H NMR spectroscopy without isolation in pure form;
DOI:10.1021/om00082a019