1,3,2-Dioxaborolane, 2-(1-chloro-2-phenylethyl)-, (S)-

Base Information

Chemical Name:1,3,2-Dioxaborolane, 2-(1-chloro-2-phenylethyl)-, (S)-
CAS No.:88765-78-0
Molecular Formula:C10H12BClO2
Molecular Weight:210.468
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3,2-Dioxaborolane, 2-(1-chloro-2-phenylethyl)-, (S)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 1,3,2-Dioxaborolane, 2-(1-chloro-2-phenylethyl)-, (S)-

There total 1 articles about 1,3,2-Dioxaborolane, 2-(1-chloro-2-phenylethyl)-, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 35895-82-0
2-benzyl-1,3,2-dioxaborolane

: 2146-67-0
(dichloromethyl)lithium

: 88765-78-0
ethylene glycol 1-chloro-2-phenylethane-1-boronate

Guidance literature:: In neat (no solvent); byproducts: LiCl; LiCH2Cl2 dissolved in the boronic ester at -100°C, kept overnight at 20°C; treated with CH2Cl2 or hexane, filtered, distilled; elem. anal.;
DOI:10.1021/ja00545a045

Reference yield: 85.0%

: 88765-78-0
ethylene glycol 1-chloro-2-phenylethane-1-boronate

: 4039-32-1
lithium hexamethyldisilazane

: 88765-79-1
ethylene glycol 1-(bis(trimethylsilyl)amino)-2-phenylethane-1-boronate

Guidance literature:: In tetrahydrofuran; byproducts: LiCl; one equiv. of boronate added to LiN(SiMe3)2 in THF at -78°C, mixt. kept overnight at 20°C; product distd. from LiCl;
DOI:10.1021/ja00407a051

Reference yield: 85.0%

: 88765-78-0
ethylene glycol 1-chloro-2-phenylethane-1-boronate

: 999-97-3
1,1,1,3,3,3-hexamethyl-disilazane

: 88765-79-1
ethylene glycol 1-(bis(trimethylsilyl)amino)-2-phenylethane-1-boronate

Guidance literature:: With n-butyllithium; In tetrahydrofuran; a soln. of (Me3Si)2NLi, prepd. from (Me3Si)2NH and BuLi in THF, was treated with the boronate at -78°C, mixt. was kept overnight; mixt. was distilled directly followed by redistn.; elem. anal.;
DOI:10.1021/om00082a019