Re₂Cl₄((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

Base Information

Chemical Name:Re₂Cl₄((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2
CAS No.:114720-23-9
Molecular Formula:C₅₂H₄₈Cl₄P₄Re₂
Molecular Weight:1311.07
Hs Code.:

Re<sub>2</sub>Cl<sub>4</sub>((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2

Synonyms:

Suppliers and Price of Re₂Cl₄((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Re₂Cl₄((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Re₂Cl₄((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

There total 5 articles about Re₂Cl₄((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 55333-37-4,199454-40-5
Re₂Cl₄(P(CH₃)3)4

: 58298-35-4,200960-40-3,114720-23-9
Re₂Cl₄((C₆H₅)2PCH₂CH₂P(C₆H₅)2)2

Guidance literature:: With C₂H₄(P(C₆H₅)2)2; In butan-1-ol; N2-atmosphere; refluxing (48 h, pptn.); filtration, washing (BuOH, Et2O), drying (vac.);

Reference yield: 33.8%

: dirhenium(II)(Cl)4(triethylphosphine)4

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 114720-23-9
α-Re2Cl4(1,2-bis(diphenylphosphino)ethane)2

Guidance literature:: In ethanol; Ar-atmosphere; refluxing Re-complex with excess phosphine for 6 d (pptn.); filtration, washing (C6H6/hexanes=1:1);
DOI:10.1016/S0020-1693(97)05726-5

Reference yield: 13.0%

: 14023-10-0
tetra-n-butylammonium octachlorodirhenate(III)

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 114720-23-9
α-Re2Cl4(1,2-bis(diphenylphosphino)ethane)2

: 33270-29-0,15628-22-5
{Re(dppe)2Cl₂}Cl

Guidance literature:: With HCl; In methanol; addn. of conc. HCl to educts in CH3OH, refluxn. 6 h, cooling to room temp., filtration of yellow green solid, washing with CH3OH, all reactions under N2; recrystn.(CH2Cl2/CH3OH), chromy. (SiO2, CH2Cl2), recrystn. (CH2Cl2/Et2O), washing with hexane/Et2O, drying, elem. anal., Nujol mull electronic absorption spectrum;