1H-Inden-1-one, 2,3-dihydro-, phenylhydrazone

Base Information

• Chemical Name: 1H-Inden-1-one, 2,3-dihydro-, phenylhydrazone
• CAS No.: 100968-91-0
• Molecular Formula: C15H14N2
• Molecular Weight: 222.29
• Mol file: 100968-91-0.mol

Synonyms:

Chemical Property of 1H-Inden-1-one, 2,3-dihydro-, phenylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Inden-1-one, 2,3-dihydro-, phenylhydrazone

There total 3 articles about 1H-Inden-1-one, 2,3-dihydro-, phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

inden-1-one (83-33-0) + phenylhydrazine (100-63-0) → 1-indanone phenylhydrazone (100968-91-0)

Guidance literature:

With acetic acid; for 0.25h; Ambient temperature;

DOI:10.1055/s-1990-27022

Reference yield:

o-phthalic dicarboxaldehyde (643-79-8) → 1-indanone phenylhydrazone (100968-91-0)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine

With pyridine;

DOI:10.1021/ja01175a054

Reference yield:

1-hydroxy-indene-2-carboxylic acid (28873-82-7) + phenylhydrazine (100-63-0) → 1-indanone phenylhydrazone (100968-91-0)

Guidance literature:

DOI:10.1021/ja01175a054

upstream raw materials:

1-hydroxy-indene-2-carboxylic acid

phenylhydrazine

inden-1-one

o-phthalic dicarboxaldehyde

Downstream raw materials:

(1-Isocyanato-indan-1-yl)-phenyl-diazene

1-Phenyl-4,5-dihydro-[1,2,4]triazolo[1,5-a]quinolin-2-one

5-benzoyl-5,10-dihydro-indeno[1,2-b]indole

C₁₆H₁₅N₃O

Refernces

• 1、 Gstach, Hubert,Seil, Patrick. "Rearrangement of 3,3-Disubstituted 1-Aryl-4,5-dihydro-5-oxo-3H-1,2,4-triazolium Tetrafluoroborates; Part 2. A Convenient Synthesis of 1,5-Annulated 1,2-Dihydro-2-phenyl-3H-1,2,4-triazol-3-ones". . p. 808 - 815. Retrieved 2007/10/02.