Technology Process of 2-hexyl-5-(-p-cyanophenyl)pyridine
There total 7 articles about 2-hexyl-5-(-p-cyanophenyl)pyridine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Raney Ni / methanol
2: bromine, Ag2SO4, H2SO4
3: N-methylpyrrolidone
With
1-methyl-pyrrolidin-2-one; sulfuric acid; bromine; silver sulfate;
nickel;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 3M sodium methoxide / pyridine
2: 1. 10percent aq. HCl; 2. 70percent HClO4 / 1. methanol; 2. glacial acetic acid
3: 42 percent / ammonium acetate / acetic acid / Heating
4: 56 percent / Raney Ni / methanol / Heating
5: 24 percent / Br2, Ag2SO4 / aq. H2SO4 / 2 h / Ambient temperature
6: various solvent(s) / Heating
With
ammonium acetate; hydrogenchloride; perchloric acid; bromine; sodium methylate; nickel; silver sulfate;
In
pyridine; methanol; sulfuric acid; acetic acid;
DOI:10.1007/BF00507095
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 3M sodium methoxide / pyridine
2: 1. 10percent aq. HCl; 2. 70percent HClO4 / 1. methanol; 2. glacial acetic acid
3: 42 percent / ammonium acetate / acetic acid / Heating
4: 56 percent / Raney Ni / methanol / Heating
5: 24 percent / Br2, Ag2SO4 / aq. H2SO4 / 2 h / Ambient temperature
6: various solvent(s) / Heating
With
ammonium acetate; hydrogenchloride; perchloric acid; bromine; sodium methylate; nickel; silver sulfate;
In
pyridine; methanol; sulfuric acid; acetic acid;
DOI:10.1007/BF00507095
