(R)-3-(4-Trifluoromethyl-benzyloxy)-octadecanoic acid ((2S,3R,4R,5S,6R)-2-allyloxy-4,5-bis-benzyloxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-amide

Base Information

Chemical Name:(R)-3-(4-Trifluoromethyl-benzyloxy)-octadecanoic acid ((2S,3R,4R,5S,6R)-2-allyloxy-4,5-bis-benzyloxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-amide
CAS No.:287922-83-2
Molecular Formula:C₄₉H₆₈F₃NO₇
Molecular Weight:840.077
Hs Code.:

(R)-3-(4-Trifluoromethyl-benzyloxy)-octadecanoic acid ((2S,3R,4R,5S,6R)-2-allyloxy-4,5-bis-benzyloxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-amide

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Chemical Property of (R)-3-(4-Trifluoromethyl-benzyloxy)-octadecanoic acid ((2S,3R,4R,5S,6R)-2-allyloxy-4,5-bis-benzyloxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-amide

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Technology Process of (R)-3-(4-Trifluoromethyl-benzyloxy)-octadecanoic acid ((2S,3R,4R,5S,6R)-2-allyloxy-4,5-bis-benzyloxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-amide

There total 5 articles about (R)-3-(4-Trifluoromethyl-benzyloxy)-octadecanoic acid ((2S,3R,4R,5S,6R)-2-allyloxy-4,5-bis-benzyloxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 287922-83-2
(R)-3-(4-Trifluoromethyl-benzyloxy)-octadecanoic acid ((2S,3R,4R,5S,6R)-2-allyloxy-4,5-bis-benzyloxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-amide

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / Ag₂O

2: 86 percent / BH₃*Me₂NH; BF₃*OEt₂ / CH₂Cl₂

3: Zn-Cu

4: WSCD*HCl; HOAt

With 1-hydroxy-7-aza-benzotriazole; dimethylamine borane; WSCD*HCl; boron trifluoride diethyl etherate; copper; silver(l) oxide; zinc; In dichloromethane; 1: benzylation / 2: Reduction / 3: Reduction / 4: Acylation;
DOI:10.1016/S0040-4039(00)01158-8

Reference yield:

: 183388-21-8
allyl 4,6-O-benzylidene-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

: 287922-83-2
(R)-3-(4-Trifluoromethyl-benzyloxy)-octadecanoic acid ((2S,3R,4R,5S,6R)-2-allyloxy-4,5-bis-benzyloxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-amide

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / Ag₂O

2: 86 percent / BH₃*Me₂NH; BF₃*OEt₂ / CH₂Cl₂

3: Zn-Cu

4: WSCD*HCl; HOAt

With 1-hydroxy-7-aza-benzotriazole; dimethylamine borane; WSCD*HCl; boron trifluoride diethyl etherate; copper; silver(l) oxide; zinc; In dichloromethane; 1: benzylation / 2: Reduction / 3: Reduction / 4: Acylation;
DOI:10.1016/S0040-4039(00)01158-8

Reference yield:

: 287922-84-3
allyl 3-O-benzyl-4,6-O-benzylidene-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

: 287922-83-2
(R)-3-(4-Trifluoromethyl-benzyloxy)-octadecanoic acid ((2S,3R,4R,5S,6R)-2-allyloxy-4,5-bis-benzyloxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / BH₃*Me₂NH; BF₃*OEt₂ / CH₂Cl₂

2: Zn-Cu

3: WSCD*HCl; HOAt

With 1-hydroxy-7-aza-benzotriazole; dimethylamine borane; WSCD*HCl; boron trifluoride diethyl etherate; copper; zinc; In dichloromethane; 1: Reduction / 2: Reduction / 3: Acylation;
DOI:10.1016/S0040-4039(00)01158-8