Technology Process of C16H15NO5S
There total 3 articles about C16H15NO5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrafluoroboric acid diethyl ether; N-iodo-succinimide / acetonitrile / -30 °C / Inert atmosphere
2: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 23 °C / Inert atmosphere
3: tetrahydrofuran / 48 h / 60 °C / aq. phosphate buffer; Inert atmosphere
With
tetrafluoroboric acid diethyl ether; N-iodo-succinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c0ob00846j
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 23 °C / Inert atmosphere
2: tetrahydrofuran / 48 h / 60 °C / aq. phosphate buffer; Inert atmosphere
With
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c0ob00846j
- Guidance literature:
-
In
tetrahydrofuran;
at 60 ℃;
for 48h;
aq. phosphate buffer;
Inert atmosphere;
DOI:10.1039/c0ob00846j