N-Methyl-2--propionanilid

Base Information

• Chemical Name: N-Methyl-2--propionanilid
• CAS No.: 46988-26-5
• Molecular Formula: C₁₄H₂₂N₂O₃
• Molecular Weight: 266.34
• Mol file: 46988-26-5.mol

Synonyms:

Chemical Property of N-Methyl-2--propionanilid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-Methyl-2--propionanilid

There total 2 articles about N-Methyl-2--propionanilid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-methylaniline (100-61-8) → N-Methyl-2--propionanilid (46988-26-5)

Guidance literature:

Multi-step reaction with 2 steps

2: K₂CO₃ / dimethylformamide

With potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1248/cpb.13.594

Reference yield:

2-bromo-N-methyl-N-phenylpropanamide (2620-11-3) + 2,2'-iminobis[ethanol] (111-42-2) → N-Methyl-2--propionanilid (46988-26-5)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1248/cpb.13.594

Reference yield:

N-Methyl-2--propionanilid (46988-26-5) → N-Methyl-2--propionsaeure-anilid (802256-19-5)

Guidance literature:

With thionyl chloride; In chloroform;

DOI:10.1248/cpb.13.594

upstream raw materials:

2-bromo-N-methyl-N-phenylpropanamide

2,2'-iminobis[ethanol]

N-methylaniline

Downstream raw materials:

N-Methyl-2--propionsaeure-anilid