9H-thioxanthene 10-oxide

Base Information

Chemical Name:9H-thioxanthene 10-oxide
CAS No.:10133-81-0
Molecular Formula:C13H10OS
Molecular Weight:214.288
Hs Code.:
DSSTox Substance ID:DTXSID00415933
Nikkaji Number:J406.348A
Wikidata:Q82225018
ChEMBL ID:CHEMBL79641
Mol file:10133-81-0.mol

Synonyms:9H-thioxanthene 10-oxide;Thioxanthen-10-oxid;9H-Thioxanthene, 10-oxide;SCHEMBL36333;10133-81-0;CHEMBL79641;DTXSID00415933;10H-dibenzo[b,e]thiopyran 5-oxide;InChI=1/C13H10OS/c14-15-12-7-3-1-5-10(12)9-11-6-2-4-8-13(11)15/h1-8H,9H

Suppliers and Price of 9H-thioxanthene 10-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 9H-thioxanthene 10-oxide

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:214.04523611
Heavy Atom Count:15
Complexity:239

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2=CC=CC=C2S(=O)C3=CC=CC=C31

Technology Process of 9H-thioxanthene 10-oxide

There total 1 articles about 9H-thioxanthene 10-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 873-66-5
1-propenylbenzene

: 94-36-0
dibenzoyl peroxide

: 65-85-0,8013-63-6
benzoic acid

: 10133-81-0
9H-thioxanthene-10-monooxide

Guidance literature:: With styrene; In acetonitrile; at 50 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c9cc09369a

Reference yield: 95.0%

: 10133-81-0
9H-thioxanthene-10-monooxide

: 261-31-4
thioxanthene

Guidance literature:: With aluminum (III) chloride; lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 1h; Reflux;
DOI:10.1246/cl.140960

Reference yield:

: 10133-81-0
9H-thioxanthene-10-monooxide

: 123168-01-4
Cyclohexyl-carbamic acid 10,10-dioxo-9,10-dihydro-10λ⁶-thioxanthen-9-ylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: aluminum (III) chloride; lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C / Reflux

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 0 - 20 °C

3: potassium hydroxide / tetrahydrofuran; methanol / 0.33 h / 0 °C

4: dibutyltin dilaurate / benzene; acetonitrile / 6 h / 20 °C

With aluminum (III) chloride; lithium aluminium tetrahydride; dibutyltin dilaurate; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; acetonitrile; benzene;
DOI:10.1246/cl.140960